6-(4-Chloro-3-methylphenyl)-4-(2,5-dimethylphenyl)-3-oxo-2,3,4,5-tetrahydropyridazine

Base Information

• Chemical Name: 6-(4-Chloro-3-methylphenyl)-4-(2,5-dimethylphenyl)-3-oxo-2,3,4,5-tetrahydropyridazine
• CAS No.: 89936-35-6
• Molecular Formula: C₁₉H₁₉ClN₂O
• Molecular Weight: 326.826

Synonyms:6-(4-Chloro-3-methylphenyl)-4-(2,5-dimethylphenyl)-3-oxo-2,3,4,5-tetrahydropyridazine

Chemical Property of 6-(4-Chloro-3-methylphenyl)-4-(2,5-dimethylphenyl)-3-oxo-2,3,4,5-tetrahydropyridazine

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Technology Process of 6-(4-Chloro-3-methylphenyl)-4-(2,5-dimethylphenyl)-3-oxo-2,3,4,5-tetrahydropyridazine

There total 1 articles about 6-(4-Chloro-3-methylphenyl)-4-(2,5-dimethylphenyl)-3-oxo-2,3,4,5-tetrahydropyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

4-(4-Chloro-3-methyl-phenyl)-2-(2,5-dimethyl-phenyl)-4-oxo-butyric acid (84587-35-9) → 6-(4-Chloro-3-methylphenyl)-4-(2,5-dimethylphenyl)-3-oxo-2,3,4,5-tetrahydropyridazine (89936-35-6)

Guidance literature:

With hydrazine hydrate; In butan-1-ol; for 5h; Heating;

DOI:10.1021/je00037a043

Reference yield: 82.0%

chloroacetic acid ethyl ester (105-39-5) + 6-(4-Chloro-3-methylphenyl)-4-(2,5-dimethylphenyl)-3-oxo-2,3,4,5-tetrahydropyridazine (89936-35-6) → [6-(4-Chloro-3-methyl-phenyl)-4-(2,5-dimethyl-phenyl)-4,5-dihydro-pyridazin-3-yloxy]-acetic acid ethyl ester (89936-39-0)

Guidance literature:

With potassium carbonate; In acetone; for 15h; Heating;

DOI:10.1021/je00037a043

Reference yield: 80.0%

6-(4-Chloro-3-methylphenyl)-4-(2,5-dimethylphenyl)-3-oxo-2,3,4,5-tetrahydropyridazine (89936-35-6) + dimethyl sulfate (77-78-1) → 6-(4-Chloro-3-methyl-phenyl)-4-(2,5-dimethyl-phenyl)-3-methoxy-4,5-dihydro-pyridazine (89936-37-8)

Guidance literature:

With potassium carbonate; In acetone; for 15h; Heating;

DOI:10.1021/je00037a043

upstream raw materials:

4-(4-Chloro-3-methyl-phenyl)-2-(2,5-dimethyl-phenyl)-4-oxo-butyric acid

Downstream raw materials:

6-(4-Chloro-3-methyl-phenyl)-4-(2,5-dimethyl-phenyl)-3-ethoxy-4,5-dihydro-pyridazine

[6-(4-Chloro-3-methyl-phenyl)-4-(2,5-dimethyl-phenyl)-4,5-dihydro-pyridazin-3-yloxy]-acetic acid ethyl ester

6-(4-Chloro-3-methyl-phenyl)-4-(2,5-dimethyl-phenyl)-2H-pyridazin-3-one

3-Chloro-6-(4-chloro-3-methyl-phenyl)-4-(2,5-dimethyl-phenyl)-4,5-dihydro-pyridazine

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