tri(o-tolyl)phosphonium tris(pentafluorophenyl)borohydride

Base Information

Chemical Name:tri(o-tolyl)phosphonium tris(pentafluorophenyl)borohydride
CAS No.:1094249-99-6
Molecular Formula:C₁₈HBF₁₅*C₂₁H₂₁P*H
Molecular Weight:818.372
Hs Code.:

Synonyms:tri(o-tolyl)phosphonium tris(pentafluorophenyl)borohydride

Suppliers and Price of tri(o-tolyl)phosphonium tris(pentafluorophenyl)borohydride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of tri(o-tolyl)phosphonium tris(pentafluorophenyl)borohydride

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of tri(o-tolyl)phosphonium tris(pentafluorophenyl)borohydride

There total 4 articles about tri(o-tolyl)phosphonium tris(pentafluorophenyl)borohydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: tri(o-tolyl)phosphonium trifluoromethanesulfonate salt

: 1109-15-5
tris(pentafluorophenyl)borate

: 1094249-99-6
tri(o-tolyl)phosphonium tris(pentafluorophenyl)borohydride

Guidance literature:: In dichloromethane; at 20 ℃; Schlenk technique; Inert atmosphere;
DOI:10.1021/acs.orglett.6b03868

Reference yield: 77.0%

: 1109-15-5
tris(pentafluorophenyl)borate

: 6163-58-2
tris-(o-tolyl)phosphine

: 1094249-99-6
tri(o-tolyl)phosphonium tris(pentafluorophenyl)borohydride

Guidance literature:: With hydrogen; In bromobenzene; at 20 ℃; under 3040.2 Torr; Inert atmosphere; Cooling with liquid nitrogen;

Reference yield:

: 95-46-5
2-methylphenyl bromide

: 1094249-99-6
tri(o-tolyl)phosphonium tris(pentafluorophenyl)borohydride

Guidance literature:: Multi-step reaction with 3 steps

1.1: magnesium / tetrahydrofuran / 0.67 h / 20 °C

1.2: 1.5 h

2.1: diethyl ether / 0.5 h / 20 °C

3.1: dichloromethane / 20 °C / Schlenk technique; Inert atmosphere

With magnesium; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/acs.orglett.6b03868