ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-5-methoxyphenylcarbamate

Base Information

• Chemical Name: ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-5-methoxyphenylcarbamate
• CAS No.: 1620090-34-7
• Molecular Formula: C₂₁H₂₃IN₂O₅S
• Molecular Weight: 542.395

Synonyms:ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-5-methoxyphenylcarbamate

Chemical Property of ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-5-methoxyphenylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-5-methoxyphenylcarbamate

There total 3 articles about ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-5-methoxyphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl-5-methoxy-2-(4-(4-methylphenylsulfonamido)but-1-ynyl)phenylcarbamate (1620090-29-0) → ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-5-methoxyphenylcarbamate (1620090-34-7)

Guidance literature:

With iodine; potassium carbonate; In acetonitrile; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1039/c4cc02466d

Reference yield:

ethyl N-(2-iodo-5-methoxyphenyl)carbamate (636567-57-2) → ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-5-methoxyphenylcarbamate (1620090-34-7)

Guidance literature:

Multi-step reaction with 2 steps

1: trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide / triethylamine / 6 h / 20 °C

2: potassium carbonate; iodine / acetonitrile / 0 - 20 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; iodine; potassium carbonate; In triethylamine; acetonitrile;

DOI:10.1039/c4cc02466d

Reference yield:

N-(but-3-yn-1-yl)-4-methylbenzenesulfonamide (161040-05-7) → ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-5-methoxyphenylcarbamate (1620090-34-7)

Guidance literature:

Multi-step reaction with 2 steps

1: trans-bis(triphenylphosphine)palladium dichloride; copper(l) iodide / triethylamine / 6 h / 20 °C

2: potassium carbonate; iodine / acetonitrile / 0 - 20 °C / Inert atmosphere

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; iodine; potassium carbonate; In triethylamine; acetonitrile;

DOI:10.1039/c4cc02466d

upstream raw materials:

ethyl N-(2-iodo-5-methoxyphenyl)carbamate

ethyl-5-methoxy-2-(4-(4-methylphenylsulfonamido)but-1-ynyl)phenylcarbamate

N-(but-3-yn-1-yl)-4-methylbenzenesulfonamide

Downstream raw materials:

ethyl-4-(2-butoxy-2-oxoethyl)-7-methoxy-1-tosyl-2,3-dihydro-1H-pyrrolo[3,2-c]quinoline-5(4H)-carboxylate

(E)-Butyl-3-(2-(2-(ethoxycarbonylamino)-4-methoxyphenyl)-1-tosyl-4,5-dihydro-1H-pyrrol-3-yl)acrylate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1620090-34-7 ethyl-2-(3-iodo-1-tosyl-4,5-dihydro-1H-pyrrol-2-yl)-5-methoxyphenylcarbamate

Send

Send

Metric Ton KG G Pound L ML

Send

Send