diethyl 2-(benzyloxycarbonyl)amino-2-[N-(1-benzyl-5-nitroimidazolyl-4-carbonyl)amino]malonate

Base Information

• Chemical Name: diethyl 2-(benzyloxycarbonyl)amino-2-[N-(1-benzyl-5-nitroimidazolyl-4-carbonyl)amino]malonate
• CAS No.: 1268388-58-4
• Molecular Formula: C₂₆H₂₇N₅O₉
• Molecular Weight: 553.528

Synonyms:diethyl 2-(benzyloxycarbonyl)amino-2-[N-(1-benzyl-5-nitroimidazolyl-4-carbonyl)amino]malonate

Chemical Property of diethyl 2-(benzyloxycarbonyl)amino-2-[N-(1-benzyl-5-nitroimidazolyl-4-carbonyl)amino]malonate

Chemical Property:

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Technology Process of diethyl 2-(benzyloxycarbonyl)amino-2-[N-(1-benzyl-5-nitroimidazolyl-4-carbonyl)amino]malonate

There total 1 articles about diethyl 2-(benzyloxycarbonyl)amino-2-[N-(1-benzyl-5-nitroimidazolyl-4-carbonyl)amino]malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

diethyl 2-amino-2-[N-(1-benzyl-5-nitroimidazolyl-4-carbonyl)amino]malonate (1268388-57-3) + benzyl chloroformate (501-53-1,94274-21-2) → diethyl 2-(benzyloxycarbonyl)amino-2-[N-(1-benzyl-5-nitroimidazolyl-4-carbonyl)amino]malonate (1268388-58-4)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Cooling with ice;

DOI:10.1016/j.bmcl.2010.11.109

Reference yield: 87.0%

diethyl 2-(benzyloxycarbonyl)amino-2-[N-(1-benzyl-5-nitroimidazolyl-4-carbonyl)amino]malonate (1268388-58-4) → diethyl 2-(benzyloxycarbonyl)amino-2-[N-(5-amino-1-benzylimidazolyl-4-carbonyl)amino]malonate (1268388-59-5)

Guidance literature:

With acetic acid; zinc; In ethanol; for 1h; Reflux;

DOI:10.1016/j.bmcl.2010.11.109

upstream raw materials:

diethyl 2-amino-2-[N-(1-benzyl-5-nitroimidazolyl-4-carbonyl)amino]malonate

benzyl chloroformate

Downstream raw materials:

diethyl 2-(benzyloxycarbonyl)amino-2-[N-(5-amino-1-benzylimidazolyl-4-carbonyl)amino]malonate

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