methyl 2,2'-anhydro-5-O-benzyl-3-deoxy-3-(thymin-1-yl)-α-D-lyxofuranoside

Base Information

Chemical Name:methyl 2,2'-anhydro-5-O-benzyl-3-deoxy-3-(thymin-1-yl)-α-D-lyxofuranoside
CAS No.:855996-19-9
Molecular Formula:C₁₈H₂₀N₂O₅
Molecular Weight:344.367
Hs Code.:

Synonyms:methyl 2,2'-anhydro-5-O-benzyl-3-deoxy-3-(thymin-1-yl)-α-D-lyxofuranoside

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Chemical Property of methyl 2,2'-anhydro-5-O-benzyl-3-deoxy-3-(thymin-1-yl)-α-D-lyxofuranoside

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Technology Process of methyl 2,2'-anhydro-5-O-benzyl-3-deoxy-3-(thymin-1-yl)-α-D-lyxofuranoside

There total 3 articles about methyl 2,2'-anhydro-5-O-benzyl-3-deoxy-3-(thymin-1-yl)-α-D-lyxofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 855996-14-4
2,2'-anhydro-5-O-benzyl-3-deoxy-3-(thymin-1-yl)-α-D-lyxofuranose

: 74-88-4
methyl iodide

: 855996-19-9
methyl 2,2'-anhydro-5-O-benzyl-3-deoxy-3-(thymin-1-yl)-α-D-lyxofuranoside

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 2h;
DOI:10.1021/ol050496v

Reference yield:

: 3,5-di-O-benzyl-2-bromo-2-deoxy-D-xylofuranose

: 855996-19-9
methyl 2,2'-anhydro-5-O-benzyl-3-deoxy-3-(thymin-1-yl)-α-D-lyxofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / DBU / dimethylformamide / 0.17 h

2: 91 percent / NaH / tetrahydrofuran / 2 h / 20 °C

With sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ol050496v

Reference yield:

: 65-71-4,28806-14-6,691841-57-3
thymin

: 855996-19-9
methyl 2,2'-anhydro-5-O-benzyl-3-deoxy-3-(thymin-1-yl)-α-D-lyxofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / DBU / dimethylformamide / 0.17 h

2: 91 percent / NaH / tetrahydrofuran / 2 h / 20 °C

With sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ol050496v