1-(3-fluorophenyl)-2-p-toluenesulfonyl ethanone

Base Information

Chemical Name:1-(3-fluorophenyl)-2-p-toluenesulfonyl ethanone
CAS No.:1486725-73-8
Molecular Formula:C₁₅H₁₃FO₃S
Molecular Weight:292.331
Hs Code.:

Synonyms:1-(3-fluorophenyl)-2-p-toluenesulfonyl ethanone

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Chemical Property of 1-(3-fluorophenyl)-2-p-toluenesulfonyl ethanone

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Technology Process of 1-(3-fluorophenyl)-2-p-toluenesulfonyl ethanone

There total 8 articles about 1-(3-fluorophenyl)-2-p-toluenesulfonyl ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1398057-04-9
1-(1-azidovinyl)-3-fluorobenzene

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1486725-73-8
1-(3-fluorophenyl)-2-p-toluenesulfonyl ethanone

Guidance literature:: 1-(1-azidovinyl)-3-fluorobenzene; toluene-4-sulfonic acid hydrazide; With tetrabutylammonium tetrafluoroborate; In water; acetonitrile; at 20 ℃; for 2h; Electrochemical reaction; Inert atmosphere; Green chemistry;

With hydrogenchloride; water; In tetrahydrofuran; at 80 ℃; for 12h; Green chemistry;
DOI:10.1002/ejoc.202001059

Reference yield: 75.0%

: 1612760-05-0
C₁₀H₁₀FNO₂

: 824-79-3
sodium 4-methylbenzenesulfinate

: 1486725-73-8
1-(3-fluorophenyl)-2-p-toluenesulfonyl ethanone

Guidance literature:: C₁₀H₁₀FNO₂; sodium 4-methylbenzenesulfinate; With copper diacetate; In dimethyl sulfoxide; at 100 ℃; for 6h; Schlenk technique; Inert atmosphere;

With silica gel; In dichloromethane; at 20 ℃;
DOI:10.1002/anie.201311217

Reference yield: 59.0%

: 2561-17-3
1-ethynyl-3-fluoro-benzene

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1486725-73-8
1-(3-fluorophenyl)-2-p-toluenesulfonyl ethanone

Guidance literature:: With tris(bipyridine)ruthenium(II) dichloride hexahydrate; oxygen; sodium acetate; potassium iodide; In water; N,N-dimethyl-formamide; at 20 ℃; under 760.051 Torr; Irradiation;
DOI:10.1039/c6ob00617e