dibenzyl 2-((tert-butoxycarbonyl)amino)-6-((R)-4-((tert-butoxycarbonyl)amino)-5-oxo-5-(undecylamino)pentanamido)heptanedioate

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Chemical Name:dibenzyl 2-((tert-butoxycarbonyl)amino)-6-((R)-4-((tert-butoxycarbonyl)amino)-5-oxo-5-(undecylamino)pentanamido)heptanedioate
CAS No.:1269619-78-4
Molecular Formula:C₄₇H₇₂N₄O₁₀
Molecular Weight:853.109
Hs Code.:

Synonyms:dibenzyl 2-((tert-butoxycarbonyl)amino)-6-((R)-4-((tert-butoxycarbonyl)amino)-5-oxo-5-(undecylamino)pentanamido)heptanedioate

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Chemical Property of dibenzyl 2-((tert-butoxycarbonyl)amino)-6-((R)-4-((tert-butoxycarbonyl)amino)-5-oxo-5-(undecylamino)pentanamido)heptanedioate

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Technology Process of dibenzyl 2-((tert-butoxycarbonyl)amino)-6-((R)-4-((tert-butoxycarbonyl)amino)-5-oxo-5-(undecylamino)pentanamido)heptanedioate

There total 15 articles about dibenzyl 2-((tert-butoxycarbonyl)amino)-6-((R)-4-((tert-butoxycarbonyl)amino)-5-oxo-5-(undecylamino)pentanamido)heptanedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 7307-55-3
1-undecylamine

: C₃₉H₅₅N₃O₁₁

: 1269619-78-4
dibenzyl 2-((tert-butoxycarbonyl)amino)-6-((R)-4-((tert-butoxycarbonyl)amino)-5-oxo-5-(undecylamino)pentanamido)heptanedioate

Guidance literature:: With dmap; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 14h;
DOI:10.1021/jm101535e

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1269619-78-4
dibenzyl 2-((tert-butoxycarbonyl)amino)-6-((R)-4-((tert-butoxycarbonyl)amino)-5-oxo-5-(undecylamino)pentanamido)heptanedioate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 1 h / 20 °C

2: Wilkinson's catalyst / ethanol; water / 3 h / 90 °C

3: dmap; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 14 h / 20 °C

With dmap; Wilkinson's catalyst; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm101535e

Reference yield:

: C₃₄H₄₅N₃O₉

: 1269619-78-4
dibenzyl 2-((tert-butoxycarbonyl)amino)-6-((R)-4-((tert-butoxycarbonyl)amino)-5-oxo-5-(undecylamino)pentanamido)heptanedioate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 1 h / 20 °C

2: Wilkinson's catalyst / ethanol; water / 3 h / 90 °C

3: dmap; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / N,N-dimethyl-formamide / 14 h / 20 °C

With dmap; Wilkinson's catalyst; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm101535e