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Technology Process of (Sn(CCC2H5CHCHCHCC2H5)2)3Sn2(1-)*N((CH2CH2O)2CH2CH2)3N*K(1+)={(Sn(CC(C2H5)(CH)3C(C2H5))2)3Sn2}{KN((CH2CH2O)2CH2CH2)3N}

(Sn(CCC2H5CHCHCHCC2H5)2)3Sn2(1-)*N((CH2CH2O)2CH2CH2)3N*K(1+)={(Sn(CC(C2H5)(CH)3C(C2H5))2)3Sn2}{KN((CH2CH2O)2CH2CH2)3N}

Base Information
  • Chemical Name:(Sn(CCC2H5CHCHCHCC2H5)2)3Sn2(1-)*N((CH2CH2O)2CH2CH2)3N*K(1+)={(Sn(CC(C2H5)(CH)3C(C2H5))2)3Sn2}{KN((CH2CH2O)2CH2CH2)3N}
  • CAS No.:130350-26-4
  • Molecular Formula:C18H36N2O6*C60H78Sn5*K
  • Molecular Weight:1808.42
  • Hs Code.:
(Sn(CCC<sub>2</sub>H<sub>5</sub>CHCHCHCC<sub>2</sub>H<sub>5</sub>)2)3Sn<sub>2</sub><sup>(1-)</sup>*N((CH<sub>2</sub>CH<sub>2</sub>O)2CH<sub>2</sub>CH<sub>2</sub>)3N*K<sup>(1+)</sup>={(Sn(CC(C<sub>2</sub>H<sub>5</sub>)(CH)3C(C<sub>2</sub>H<sub>5</sub>))2)3Sn<sub>2</sub>}{KN((CH<sub>2</sub>CH<sub>2</sub>O)2CH<sub>2</sub>CH<sub>2</sub>)3N}

Synonyms:(Sn(CCC2H5CHCHCHCC2H5)2)3Sn2(1-)*N((CH2CH2O)2CH2CH2)3N*K(1+)={(Sn(CC(C2H5)(CH)3C(C2H5))2)3Sn2}{KN((CH2CH2O)2CH2CH2)3N}

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Chemical Property of (Sn(CCC2H5CHCHCHCC2H5)2)3Sn2(1-)*N((CH2CH2O)2CH2CH2)3N*K(1+)={(Sn(CC(C2H5)(CH)3C(C2H5))2)3Sn2}{KN((CH2CH2O)2CH2CH2)3N}
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Technology Process of (Sn(CCC2H5CHCHCHCC2H5)2)3Sn2(1-)*N((CH2CH2O)2CH2CH2)3N*K(1+)={(Sn(CC(C2H5)(CH)3C(C2H5))2)3Sn2}{KN((CH2CH2O)2CH2CH2)3N}

There total 1 articles about (Sn(CCC2H5CHCHCHCC2H5)2)3Sn2(1-)*N((CH2CH2O)2CH2CH2)3N*K(1+)={(Sn(CC(C2H5)(CH)3C(C2H5))2)3Sn2}{KN((CH2CH2O)2CH2CH2)3N} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

hexakis(2,6-diethylphenyl)pentastanna{1.1.1}propellane
122115-73-5

hexakis(2,6-diethylphenyl)pentastanna{1.1.1}propellane

[2.2.2]cryptande
23978-09-8

[2.2.2]cryptande

(Sn(CCC<sub>2</sub>H<sub>5</sub>CHCHCHCC<sub>2</sub>H<sub>5</sub>)2)3Sn<sub>2</sub><sup>(1-)</sup>*N((CH<sub>2</sub>CH<sub>2</sub>O)2CH<sub>2</sub>CH<sub>2</sub>)3N*K<sup>(1+)</sup>={(Sn(CC(C<sub>2</sub>H<sub>5</sub>)(CH)3C(C<sub>2</sub>H<sub>5</sub>))2)3Sn<sub>2</sub>}{KN((CH<sub>2</sub>CH<sub>2</sub>O)2CH<sub>2</sub>CH<sub>2</sub>)3N}
130350-26-4

(Sn(CCC2H5CHCHCHCC2H5)2)3Sn2(1-)*N((CH2CH2O)2CH2CH2)3N*K(1+)={(Sn(CC(C2H5)(CH)3C(C2H5))2)3Sn2}{KN((CH2CH2O)2CH2CH2)3N}

Guidance literature:
With potassium amalgam; In toluene; under N2 or Ar, standard Schlenk techniques, addn. of cryptand and potassium amalgam to a soln. of complex in toluene, stirred for 30 min, left to stand for 30 min, reversible react. with SnCl2; decantation, dissolved in 1,2-dimethoxyethane, addn. of toluene, stored at -40°C, after 7 d pptn., washed with cooled hexane at-40°C, dried in vac.;
DOI:10.1021/ja00180a027
upstream raw materials:

hexakis(2,6-diethylphenyl)pentastanna{1.1.1}propellane

[2.2.2]cryptande

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