9-(4-(4-(2,5-diiodo-4-methoxyphenoxy)butoxy)phenyl)-10-phenylanthracene

Base Information

Chemical Name:9-(4-(4-(2,5-diiodo-4-methoxyphenoxy)butoxy)phenyl)-10-phenylanthracene
CAS No.:1277104-05-8
Molecular Formula:C₃₇H₃₀I₂O₃
Molecular Weight:776.452
Hs Code.:

Synonyms:9-(4-(4-(2,5-diiodo-4-methoxyphenoxy)butoxy)phenyl)-10-phenylanthracene

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Chemical Property of 9-(4-(4-(2,5-diiodo-4-methoxyphenoxy)butoxy)phenyl)-10-phenylanthracene

Chemical Property:

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Technology Process of 9-(4-(4-(2,5-diiodo-4-methoxyphenoxy)butoxy)phenyl)-10-phenylanthracene

There total 4 articles about 9-(4-(4-(2,5-diiodo-4-methoxyphenoxy)butoxy)phenyl)-10-phenylanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1109215-59-9
1-(4-bromobutoxy)-2,5-diiodo-4-methoxybenzene

: 192872-06-3
9-(4-hydroxyphenyl)-10-(phenyl)anthracene

: 1277104-05-8
9-(4-(4-(2,5-diiodo-4-methoxyphenoxy)butoxy)phenyl)-10-phenylanthracene

Guidance literature:: With potassium carbonate; In butanone; at 80 ℃; Inert atmosphere;
DOI:10.1039/c0cc05770c

Reference yield:

: 23674-20-6
9-bromo-10-phenylanthracene

: 1277104-05-8
9-(4-(4-(2,5-diiodo-4-methoxyphenoxy)butoxy)phenyl)-10-phenylanthracene

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; Aliquat 336; potassium carbonate / water; toluene / 90 °C / Inert atmosphere

2: phosphorus tribromide / dichloromethane / -78 - 20 °C

3: potassium carbonate / butanone / 80 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphorus tribromide; Aliquat 336; potassium carbonate; In dichloromethane; water; toluene; butanone; 1: Suzuki coupling;
DOI:10.1039/c0cc05770c

Reference yield:

: 602-55-1
9-phenylanthracene

: 1277104-05-8
9-(4-(4-(2,5-diiodo-4-methoxyphenoxy)butoxy)phenyl)-10-phenylanthracene

Guidance literature:: Multi-step reaction with 4 steps

1: bromine / dichloromethane / 20 °C

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; Aliquat 336; potassium carbonate / water; toluene / 90 °C / Inert atmosphere

3: phosphorus tribromide / dichloromethane / -78 - 20 °C

4: potassium carbonate / butanone / 80 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; phosphorus tribromide; Aliquat 336; potassium carbonate; In dichloromethane; water; toluene; butanone; 2: Suzuki coupling;
DOI:10.1039/c0cc05770c