C₁₆H₁₅NO₄

Base Information

• Chemical Name: C₁₆H₁₅NO₄
• CAS No.: 1359764-17-2
• Molecular Formula: C₁₆H₁₅NO₄
• Molecular Weight: 285.299
• Mol file: 1359764-17-2.mol

Synonyms:C₁₆H₁₅NO₄

Chemical Property of C₁₆H₁₅NO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₁₅NO₄

There total 2 articles about C₁₆H₁₅NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diphenylether (101-84-8) → C16H15NO4 (1359764-17-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: aluminum (III) chloride / dichloromethane / 20 °C / Inert atmosphere

1.2: 5 - 20 °C / Inert atmosphere

2.1: hydroxylamine hydrochloride / ethanol / Reflux

With aluminum (III) chloride; hydroxylamine hydrochloride; In ethanol; dichloromethane; 1.1: Friedel Crafts acylation / 1.2: Friedel Crafts acylation;

DOI:10.1021/jf204778v

Reference yield:

ethyl 2-oxo-2-(4-phenoxyphenyl)acetate (62936-33-8) → C16H15NO4 (1359764-17-2)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; Reflux;

DOI:10.1021/jf204778v

Reference yield: 58.0%

C16H15NO4 (1359764-17-2) → 2-amino-2-(4-phenoxyphenyl)ethanol (1177277-27-8)

Guidance literature:

C₁₆H₁₅NO₄; With sodium tetrahydroborate; iodine; In tetrahydrofuran; Reflux;

With sodium hydroxide; at 100 ℃;

DOI:10.1021/jf204778v

upstream raw materials:

diphenylether

ethyl 2-oxo-2-(4-phenoxyphenyl)acetate

Downstream raw materials:

2-amino-2-(4-phenoxyphenyl)ethanol

C₂₁H₂₂ClN₃O₃

C₂₁H₂₃N₃O₃

C₂₁H₂₁Cl₂N₃O₂