1-(2,3-dideoxy-5-O-p-toluoyl-β-D-glycero-pentofuranosyl)-6,7-dimethyllumazine

Base Information

Chemical Name:1-(2,3-dideoxy-5-O-p-toluoyl-β-D-glycero-pentofuranosyl)-6,7-dimethyllumazine
CAS No.:159228-05-4
Molecular Formula:C₂₁H₂₂N₄O₅
Molecular Weight:410.429
Hs Code.:

Synonyms:1-(2,3-dideoxy-5-O-p-toluoyl-β-D-glycero-pentofuranosyl)-6,7-dimethyllumazine

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Chemical Property of 1-(2,3-dideoxy-5-O-p-toluoyl-β-D-glycero-pentofuranosyl)-6,7-dimethyllumazine

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Technology Process of 1-(2,3-dideoxy-5-O-p-toluoyl-β-D-glycero-pentofuranosyl)-6,7-dimethyllumazine

There total 6 articles about 1-(2,3-dideoxy-5-O-p-toluoyl-β-D-glycero-pentofuranosyl)-6,7-dimethyllumazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 159228-04-3
1-(2,3-dideoxy-3-iodo-5-O-p-toluoyl-β-D-erythro-pentofuranosyl)-6,7-dimethyllumazine

: 159228-05-4
1-(2,3-dideoxy-5-O-p-toluoyl-β-D-glycero-pentofuranosyl)-6,7-dimethyllumazine

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 85 ℃; for 2h;
DOI:10.1080/15257779408013278

Reference yield:

: 50256-07-0
1-[O³,O⁵-bis-(4-methyl-benzoyl)-β-D-erythro-2-deoxy-pentofuranosyl]-6,7-dimethyl-1H-pteridine-2,4-dione

: 159228-05-4
1-(2,3-dideoxy-5-O-p-toluoyl-β-D-glycero-pentofuranosyl)-6,7-dimethyllumazine

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / NaOCH₃ / 2 h / Ambient temperature

2: 73 percent / pyridine; 1,2-dichloro-ethane

3: 72 percent / methyltriphenoxyphosphonium iodide / dimethylformamide / 2 h / Ambient temperature

4: 82 percent / AIBN, n-Bu₃SnH / toluene / 2 h / 85 °C

With 2,2'-azobis(isobutyronitrile); methyltriphenoxyphosphonium iodide; tri-n-butyl-tin hydride; sodium methylate; In pyridine; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
DOI:10.1080/15257779408013278

Reference yield:

: 35777-72-1
1-(2-deoxy-β-D-erythro-pentofuranosyl)-6,7-dimethyllumazine

: 159228-05-4
1-(2,3-dideoxy-5-O-p-toluoyl-β-D-glycero-pentofuranosyl)-6,7-dimethyllumazine

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / pyridine; 1,2-dichloro-ethane

2: 72 percent / methyltriphenoxyphosphonium iodide / dimethylformamide / 2 h / Ambient temperature

3: 82 percent / AIBN, n-Bu₃SnH / toluene / 2 h / 85 °C

With 2,2'-azobis(isobutyronitrile); methyltriphenoxyphosphonium iodide; tri-n-butyl-tin hydride; In pyridine; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
DOI:10.1080/15257779408013278