diethyl N,N'-[2-[[3,5-dichloro-4-(1-cyano-1-methylethyl)phenyl]hydrazono]-1,3-dioxo-1,3-propanediyl]dicarbamate

Base Information

• Chemical Name: diethyl N,N'-[2-[[3,5-dichloro-4-(1-cyano-1-methylethyl)phenyl]hydrazono]-1,3-dioxo-1,3-propanediyl]dicarbamate
• CAS No.: 261512-56-5
• Molecular Formula: C₁₉H₂₁Cl₂N₅O₆
• Molecular Weight: 486.312

Synonyms:diethyl N,N'-[2-[[3,5-dichloro-4-(1-cyano-1-methylethyl)phenyl]hydrazono]-1,3-dioxo-1,3-propanediyl]dicarbamate

Chemical Property of diethyl N,N'-[2-[[3,5-dichloro-4-(1-cyano-1-methylethyl)phenyl]hydrazono]-1,3-dioxo-1,3-propanediyl]dicarbamate

Chemical Property:

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Technology Process of diethyl N,N'-[2-[[3,5-dichloro-4-(1-cyano-1-methylethyl)phenyl]hydrazono]-1,3-dioxo-1,3-propanediyl]dicarbamate

There total 5 articles about diethyl N,N'-[2-[[3,5-dichloro-4-(1-cyano-1-methylethyl)phenyl]hydrazono]-1,3-dioxo-1,3-propanediyl]dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

malonyldiurethane (49754-15-6) + 4-amino-2,6-dichloro-α,α-dimethylbenzeneacetonitrile (261512-48-5) → diethyl N,N'-[2-[[3,5-dichloro-4-(1-cyano-1-methylethyl)phenyl]hydrazono]-1,3-dioxo-1,3-propanediyl]dicarbamate (261512-56-5)

Guidance literature:

4-amino-2,6-dichloro-α,α-dimethylbenzeneacetonitrile; With hydrogenchloride; acetic acid; sodium nitrite; at 10 ℃; for 1.83333h;

malonyldiurethane; With sodium acetate; for 0.666667h;

DOI:10.1021/jm049479m

Reference yield:

diethyl(1,3-dioxo-1,3-propanediyl)biscarbamate + 4-amino-2,6-dichloro-α,α-dimethylbenzeneacetonitrile (261512-48-5) → diethyl N,N'-[2-[[3,5-dichloro-4-(1-cyano-1-methylethyl)phenyl]hydrazono]-1,3-dioxo-1,3-propanediyl]dicarbamate (261512-56-5)

Guidance literature:

With hydrogenchloride; sodium acetate; sodium nitrite; In water; acetic acid;

Reference yield:

2-[3,5-di-chloro4-[1-[4-(3-chlorophenyl)-5-methyl-2-thiazolyl]-1-methylethyl]phenyl]-1,2,4-triazine-3,5(2H,4H)-dione + diethyl(1,3-dioxo-1,3-propanediyl)biscarbamate → diethyl N,N'-[2-[[3,5-dichloro-4-(1-cyano-1-methylethyl)phenyl]hydrazono]-1,3-dioxo-1,3-propanediyl]dicarbamate (261512-56-5)

Guidance literature:

With hydrogenchloride; sodium acetate; sodium nitrite; In water; acetic acid;

upstream raw materials:

malonyldiurethane

4-amino-2,6-dichloro-α,α-dimethylbenzeneacetonitrile

2,6-dichloro-α,α-dimethyl-4-nitrobenzeneacetonitrile

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