(S)-4-((1S,2S)-2-Benzenesulfonyl-4-methylene-cyclopentyl)-2,2-dimethyl-[1,3]dioxolane

Base Information

Chemical Name:(S)-4-((1S,2S)-2-Benzenesulfonyl-4-methylene-cyclopentyl)-2,2-dimethyl-[1,3]dioxolane
CAS No.:123538-55-6
Molecular Formula:C₁₇H₂₂O₄S
Molecular Weight:322.425
Hs Code.:

Synonyms:(S)-4-((1S,2S)-2-Benzenesulfonyl-4-methylene-cyclopentyl)-2,2-dimethyl-[1,3]dioxolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-4-((1S,2S)-2-Benzenesulfonyl-4-methylene-cyclopentyl)-2,2-dimethyl-[1,3]dioxolane

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Technology Process of (S)-4-((1S,2S)-2-Benzenesulfonyl-4-methylene-cyclopentyl)-2,2-dimethyl-[1,3]dioxolane

There total 4 articles about (S)-4-((1S,2S)-2-Benzenesulfonyl-4-methylene-cyclopentyl)-2,2-dimethyl-[1,3]dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56069-39-7
diethyl phenylsulfonylmethylphosphonate

: 123488-10-8,123538-54-5,123538-55-6
(R)-4-((1S,2R)-2-Benzenesulfonyl-4-methylene-cyclopentyl)-2,2-dimethyl-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / t-C₄H₉OK / tetrahydrofuran / 2 h / -78 °C

2: Pd(OAc)2, (i-C₃H₇O)3P / toluene / 1.5 h / 80 °C

With potassium tert-butylate; palladium diacetate; triisopropyl phosphite; In tetrahydrofuran; toluene;
DOI:10.1021/ja00201a032

Reference yield:

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 123488-10-8,123538-54-5,123538-55-6
(R)-4-((1S,2R)-2-Benzenesulfonyl-4-methylene-cyclopentyl)-2,2-dimethyl-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / t-C₄H₉OK / tetrahydrofuran / 2 h / -78 °C

2: Pd(OAc)2, (i-C₃H₇O)3P / toluene / 1.5 h / 80 °C

With potassium tert-butylate; palladium diacetate; triisopropyl phosphite; In tetrahydrofuran; toluene;
DOI:10.1021/ja00201a032

Reference yield:

: 72047-94-0
[2-(acetoxymethyl)prop-2-enyl]trimethylsilane

: 123538-50-1
3(S),4-Dihydroxy-1-(phenylsulfonyl)-(E)-1-butene acetonide

: 123488-10-8
(S)-4-((1S,2R)-2-Benzenesulfonyl-4-methylene-cyclopentyl)-2,2-dimethyl-[1,3]dioxolane

: 123488-10-8,123538-54-5,123538-55-6
(R)-4-((1S,2R)-2-Benzenesulfonyl-4-methylene-cyclopentyl)-2,2-dimethyl-[1,3]dioxolane

Guidance literature:: palladium diacetate; triisopropyl phosphite; In toluene; at 80 ℃; for 1.5h; Yield given. Yields of byproduct given;
DOI:10.1021/ja00201a032