N-benzyl-N-(3-(N-(2-methoxyphenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide

Base Information

Chemical Name:N-benzyl-N-(3-(N-(2-methoxyphenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide
CAS No.:1606142-72-6
Molecular Formula:C₂₉H₂₆N₆O₁₃S₂
Molecular Weight:730.69
Hs Code.:

Synonyms:N-benzyl-N-(3-(N-(2-methoxyphenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide

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Chemical Property of N-benzyl-N-(3-(N-(2-methoxyphenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide

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Technology Process of N-benzyl-N-(3-(N-(2-methoxyphenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide

There total 4 articles about N-benzyl-N-(3-(N-(2-methoxyphenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 303755-57-9
N-(2-methoxyphenyl)-2,4-dinitrobenzenesulfonamide

: N-benzyl-N-(3-hydroxypropyl)-2,4-dinitrobenzenesulfonamide

: 1606142-72-6
N-benzyl-N-(3-(N-(2-methoxyphenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In toluene; at 0 - 20 ℃;
DOI:10.1016/j.bmcl.2015.04.046

Reference yield:

: 100-39-0
benzyl bromide

: 1606142-72-6
N-benzyl-N-(3-(N-(2-methoxyphenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 20 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 0 - 20 °C

With di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; toluene; 2: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2015.04.046

Reference yield:

: 1656-44-6
2,4-dinitrobenzenesulfonyl chloride

: 1606142-72-6
N-benzyl-N-(3-(N-(2-methoxyphenyl)-2,4-dinitrophenylsulfonamido)propyl)-2,4-dinitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / dichloromethane / -78 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3: triphenylphosphine; di-isopropyl azodicarboxylate / toluene / 0 - 20 °C

With pyridine; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide; toluene; 3: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2015.04.046