Technology Process of C33H38BrN6O9PS
There total 8 articles about C33H38BrN6O9PS which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
dmap;
In
N,N-dimethyl-formamide;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine; bromobenzene / potassium iodide / acetone
1.3: 760.05 Torr
2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dmap / N,N-dimethyl-formamide / 20 °C
With
bromobenzene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
dmap; potassium iodide;
In
N,N-dimethyl-formamide; acetone;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: caesium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C
2.1: tetrahydrofuran; methanol / 20 °C / NaOAc-AcOH buffer
2.2: 2 h / 20 °C
3.1: silver carbonate / N,N-dimethyl-formamide / 100 °C
4.1: bromine / acetic acid / 1 h / 20 °C
4.2: 1 h
5.1: triethylamine / dichloromethane; tetrahydrofuran / 20 °C
5.2: 6 h
6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dmap / N,N-dimethyl-formamide / 20 °C
With
bromine; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; silver carbonate;
dmap;
In
tetrahydrofuran; methanol; dichloromethane; acetic acid; N,N-dimethyl-formamide;