(+/-)-O-allyl 3-hydroxy-2-(hydroxyphenyl)methylbutanohydroxamate

Base Information

Chemical Name:(+/-)-O-allyl 3-hydroxy-2-(hydroxyphenyl)methylbutanohydroxamate
CAS No.:236737-62-5
Molecular Formula:C₁₄H₁₉NO₄
Molecular Weight:265.309
Hs Code.:

Synonyms:(+/-)-O-allyl 3-hydroxy-2-(hydroxyphenyl)methylbutanohydroxamate

Suppliers and Price of (+/-)-O-allyl 3-hydroxy-2-(hydroxyphenyl)methylbutanohydroxamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-O-allyl 3-hydroxy-2-(hydroxyphenyl)methylbutanohydroxamate

Chemical Property:

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Technology Process of (+/-)-O-allyl 3-hydroxy-2-(hydroxyphenyl)methylbutanohydroxamate

There total 3 articles about (+/-)-O-allyl 3-hydroxy-2-(hydroxyphenyl)methylbutanohydroxamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 236737-62-5
(+/-)-O-allyl 3-hydroxy-2-(hydroxyphenyl)methylbutanohydroxamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) hexane, THF, -78 deg C, 1 h, 2.) hexane, THF, -78 deg C, 3.5 h

2: 1M aq. NaOH / tetrahydrofuran / 2 h / Ambient temperature

3: aq. HCl, EDC*HCl

With hydrogenchloride; sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1021/ja990400q

Reference yield:

: 236754-26-0
(+/-)-methyl 3-hydroxy-2-<(1-hydroxy-1-phenyl)methyl>butanoate

: 236737-62-5
(+/-)-O-allyl 3-hydroxy-2-(hydroxyphenyl)methylbutanohydroxamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1M aq. NaOH / tetrahydrofuran / 2 h / Ambient temperature

2: aq. HCl, EDC*HCl

With hydrogenchloride; sodium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran;
DOI:10.1021/ja990400q

Reference yield:

: 38945-21-0
O-allylhydroxylamine hydrochloride

: 3-hydroxy-2-(hydroxy-phenyl-methyl)-butyric acid

: 236737-62-5
(+/-)-O-allyl 3-hydroxy-2-(hydroxyphenyl)methylbutanohydroxamate

Guidance literature:: With hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; Yield given;
DOI:10.1021/ja990400q