phenyl 3-allyloxycarbonylamino-4-O-acetyl-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

Base Information

Chemical Name:phenyl 3-allyloxycarbonylamino-4-O-acetyl-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside
CAS No.:849071-44-9
Molecular Formula:C₁₈H₂₃NO₅S
Molecular Weight:365.45
Hs Code.:

Synonyms:phenyl 3-allyloxycarbonylamino-4-O-acetyl-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

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Chemical Property of phenyl 3-allyloxycarbonylamino-4-O-acetyl-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

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Technology Process of phenyl 3-allyloxycarbonylamino-4-O-acetyl-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

There total 4 articles about phenyl 3-allyloxycarbonylamino-4-O-acetyl-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 849071-48-3
phenyl 3-allyloxycarbonylamino-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

: 108-24-7
acetic anhydride

: 849071-44-9
phenyl 3-allyloxycarbonylamino-4-O-acetyl-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.tetasy.2004.12.006

Reference yield:

: 849071-47-2
phenyl 3-azido-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

: 849071-44-9
phenyl 3-allyloxycarbonylamino-4-O-acetyl-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: PPh₃; H₂O / tetrahydrofuran / 2 h / 60 °C

2: 770 mg / tetrahydrofuran; H₂O / 3 h / 20 °C

3: 97 percent / triethylamine; DMAP / CH₂Cl₂ / 1 h / 20 °C

With dmap; water; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; water; 1: Staudinger reduction;
DOI:10.1016/j.tetasy.2004.12.006

Reference yield:

: (2S,3S,4S)-4-Amino-2-methyl-6-phenylsulfanyl-tetrahydro-pyran-3-ol

: 849071-44-9
phenyl 3-allyloxycarbonylamino-4-O-acetyl-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 770 mg / tetrahydrofuran; H₂O / 3 h / 20 °C

2: 97 percent / triethylamine; DMAP / CH₂Cl₂ / 1 h / 20 °C

With dmap; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tetasy.2004.12.006