phenyl 3-allyloxycarbonylamino-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

Base Information

Chemical Name:phenyl 3-allyloxycarbonylamino-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside
CAS No.:849071-48-3
Molecular Formula:C₁₆H₂₁NO₄S
Molecular Weight:323.413
Hs Code.:

Synonyms:phenyl 3-allyloxycarbonylamino-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

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Chemical Property of phenyl 3-allyloxycarbonylamino-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

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Technology Process of phenyl 3-allyloxycarbonylamino-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

There total 3 articles about phenyl 3-allyloxycarbonylamino-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 849071-47-2
phenyl 3-azido-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

: 849071-48-3
phenyl 3-allyloxycarbonylamino-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: PPh₃; H₂O / tetrahydrofuran / 2 h / 60 °C

2: 770 mg / tetrahydrofuran; H₂O / 3 h / 20 °C

With water; triphenylphosphine; In tetrahydrofuran; water; 1: Staudinger reduction;
DOI:10.1016/j.tetasy.2004.12.006

Reference yield:

: 755033-91-1
phenyl 4-O-acetyl-3-azido-1-thio-2,3,6-trideoxy-α/β-L-lyxo-hexopyranoside

: 849071-48-3
phenyl 3-allyloxycarbonylamino-2,3,6-trideoxy-1-thio-L-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / MeOH; K₂CO₃ / 8 h

2: PPh₃; H₂O / tetrahydrofuran / 2 h / 60 °C

3: 770 mg / tetrahydrofuran; H₂O / 3 h / 20 °C

With methanol; water; potassium carbonate; triphenylphosphine; In tetrahydrofuran; water; 2: Staudinger reduction;
DOI:10.1016/j.tetasy.2004.12.006