4-(2-Benzyloxycarbonylamino-3-oxo-3-pyrrolidin-1-yl-propyl)-thiobenzimidic acid methyl ester; hydriodide

Base Information

Chemical Name:4-(2-Benzyloxycarbonylamino-3-oxo-3-pyrrolidin-1-yl-propyl)-thiobenzimidic acid methyl ester; hydriodide
CAS No.:101514-65-2
Molecular Formula:C₂₃H₂₇N₃O₃S*HI
Molecular Weight:553.464
Hs Code.:

Synonyms:4-(2-Benzyloxycarbonylamino-3-oxo-3-pyrrolidin-1-yl-propyl)-thiobenzimidic acid methyl ester; hydriodide

Suppliers and Price of 4-(2-Benzyloxycarbonylamino-3-oxo-3-pyrrolidin-1-yl-propyl)-thiobenzimidic acid methyl ester; hydriodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2-Benzyloxycarbonylamino-3-oxo-3-pyrrolidin-1-yl-propyl)-thiobenzimidic acid methyl ester; hydriodide

Chemical Property:

Purity/Quality:: 99% ，98% ^*data from raw suppliers

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Technology Process of 4-(2-Benzyloxycarbonylamino-3-oxo-3-pyrrolidin-1-yl-propyl)-thiobenzimidic acid methyl ester; hydriodide

There total 6 articles about 4-(2-Benzyloxycarbonylamino-3-oxo-3-pyrrolidin-1-yl-propyl)-thiobenzimidic acid methyl ester; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 101514-61-8
[2-Oxo-2-pyrrolidin-1-yl-1-(4-thiocarbamoyl-benzyl)-ethyl]-carbamic acid benzyl ester

: 74-88-4
methyl iodide

: 101514-65-2
4-(2-Benzyloxycarbonylamino-3-oxo-3-pyrrolidin-1-yl-propyl)-thiobenzimidic acid methyl ester; hydriodide

Guidance literature:: In acetone; for 0.166667h; Heating;

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 101514-65-2
4-(2-Benzyloxycarbonylamino-3-oxo-3-pyrrolidin-1-yl-propyl)-thiobenzimidic acid methyl ester; hydriodide

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / NaOH

2: 85 percent / DDC / pyridine / 1.) 2 h, 2.) room temp., 1 d

3: 80 percent / pyridine / 12 h / Ambient temperature

4: 90 percent / H₂S (gas), TEA / pyridine / 48 h / Ambient temperature

5: 80 percent / acetone / 0.17 h / Heating

With pyridine; sodium hydroxide; TEA; hydrogen sulfide; 2`,3`-dideoxycytidine; In pyridine; acetone;

Reference yield:

: 101514-54-9
N-<(benzyloxy)carbonyl>-3-(p-cyanophenyl)-D,L-alanine

: 101514-65-2
4-(2-Benzyloxycarbonylamino-3-oxo-3-pyrrolidin-1-yl-propyl)-thiobenzimidic acid methyl ester; hydriodide

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / DDC / pyridine / 1.) 2 h, 2.) room temp., 1 d

2: 80 percent / pyridine / 12 h / Ambient temperature

3: 90 percent / H₂S (gas), TEA / pyridine / 48 h / Ambient temperature

4: 80 percent / acetone / 0.17 h / Heating

With pyridine; TEA; hydrogen sulfide; 2`,3`-dideoxycytidine; In pyridine; acetone;