1-phenyl-1,4-dibromobutane

Base Information

• Chemical Name: 1-phenyl-1,4-dibromobutane
• CAS No.: 71052-93-2
• Molecular Formula: C₁₀H₁₂Br₂
• Molecular Weight: 292.013
• Mol file: 71052-93-2.mol

Synonyms:1-phenyl-1,4-dibromobutane

Chemical Property of 1-phenyl-1,4-dibromobutane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-phenyl-1,4-dibromobutane

There total 6 articles about 1-phenyl-1,4-dibromobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

tetrahydro-2-phenylfuran (16133-83-8) → 1-phenyl-1,4-dibromobutane (71052-93-2) + C10H14BrO3P

Guidance literature:

With hydrogen bromide; phosphorus tribromide; at 0 ℃; for 0.666667h;

DOI:10.1007/BF00954229

Reference yield:

1-phenyl-butane-1,4-diol (4850-50-4) → 1-phenyl-1,4-dibromobutane (71052-93-2)

Guidance literature:

With chloroform; phosphorus pentabromide;

Reference yield:

1-Phenyl-3-buten-1-ol (80735-94-0,936-58-3) → 1-phenyl-1,4-dibromobutane (71052-93-2)

Guidance literature:

With hydrogen bromide; im Quarzgefaess bei Bestrahlung durch Sonnenlicht;

upstream raw materials:

1-Phenyl-3-buten-1-ol

1-phenyl-butane-1,4-diol

tetrahydro-2-phenylfuran

hydrogen bromide

Downstream raw materials:

acide phenyl-2 cyclopentanedicarboxylique-1,1

methyl trans-1,2-diphenylcyclopentane-1-carboxylate

methyl cis-1,2-diphenylcyclopentane-1-carboxylate

diphenyl-1,2 cyclopentanecarbonitrile-1 cis

Refernces

• 1、 Doering, W. von E.,Birladeanu, Ludmila. "Retention of Chirality during Thermal Automerization of Methyl 1,2-Diphenylcyclopentane-1-carboxylate". . p. 7461 - 7462. Retrieved 2007/10/02.