3-[(Methylamino)methyl]phenylmethanol

Base Information

Chemical Name:3-[(Methylamino)methyl]phenylmethanol
CAS No.:69383-73-9
Molecular Formula:C₉H₁₃NO
Molecular Weight:151.208
Hs Code.:
DSSTox Substance ID:DTXSID901283030

Synonyms:3-[(Methylamino)methyl]phenylmethanol;69383-73-9;SCHEMBL7026536;GDMUNGBYFQGLBW-UHFFFAOYSA-N;DTXSID901283030;AKOS015968212;3-[(Methylamino)methyl]benzenemethanol

Suppliers and Price of 3-[(Methylamino)methyl]phenylmethanol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 3-[(Methylamino)methyl]phenylmethanol

Chemical Property:

XLogP3:0.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:151.099714038
Heavy Atom Count:11
Complexity:106

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CNCC1=CC(=CC=C1)CO

Technology Process of 3-[(Methylamino)methyl]phenylmethanol

There total 4 articles about 3-[(Methylamino)methyl]phenylmethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 23668-00-0
3-(N-methylaminocarbonyl)benzoic acid methyl ester

: 69383-73-9
3-(N-methylaminomethyl)-benzenemethanol

Guidance literature:: 3-(N-methylaminocarbonyl)benzoic acid methyl ester; With lithium aluminium tetrahydride; In tetrahydrofuran; Reflux;

With sodium hydroxide; In tetrahydrofuran; water;
DOI:10.1039/c6dt01212d

Reference yield:

: 1877-71-0
benzene 1,3-dicarboxylic acid monomethyl ester

: 69383-73-9
3-(N-methylaminomethyl)-benzenemethanol

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1.5 h / Reflux

2: tetrahydrofuran / 0 - 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / Reflux

With lithium aluminium tetrahydride; oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c6dt01212d

Reference yield:

: 3441-03-0
3-(methoxycarbonyl)benzoyl chloride

: 69383-73-9
3-(N-methylaminomethyl)-benzenemethanol

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0 - 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / Reflux

With lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1039/c6dt01212d