phenyl 2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-1-thio-β-D-glucopranoside

Base Information

• Chemical Name: phenyl 2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-1-thio-β-D-glucopranoside
• CAS No.: 213012-40-9
• Molecular Formula: C₆₀H₆₂O₁₀S
• Molecular Weight: 975.212

Synonyms:phenyl 2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-1-thio-β-D-glucopranoside

Chemical Property of phenyl 2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-1-thio-β-D-glucopranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenyl 2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-1-thio-β-D-glucopranoside

There total 2 articles about phenyl 2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-1-thio-β-D-glucopranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-glucopranosyl-[1-4]-2,3,6-tri-O-benzyl-1-thio-β-D-glucopranoside (895576-74-6) → phenyl 2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-1-thio-β-D-glucopranoside (213012-40-9)

Guidance literature:

With chloro-trimethyl-silane; 4 A molecular sieve; sodium cyanoborohydride; In acetonitrile; at 20 ℃; for 5h;

Reference yield:

phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside (87470-76-6) → phenyl 2,3,6,2',3',4'-hexa-O-benzyl-1-thio-β-cellobioside (87470-77-7) + phenyl 2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-1-thio-β-D-glucopranoside (213012-40-9)

Guidance literature:

With aluminium trichloride; trimethylamine-borane; In dichloromethane;

DOI:10.1016/S0040-4039(98)01176-9

Reference yield: 90.0%

acetic anhydride (108-24-7) + phenyl 2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-1-thio-β-D-glucopranoside (213012-40-9) → phenyl(4-O-acetyl-2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-[1-4]-2,3,6-tri-O-benzyl-1-thio-D-glucopyranoside (895576-75-7)

Guidance literature:

With pyridine; at 20 ℃;

upstream raw materials:

phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-glucopyranosyl-(1→4)-2,3,6-tri-O-benzyl-1-thio-β-D-glucopyranoside

phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-β-D-glucopranosyl-[1-4]-2,3,6-tri-O-benzyl-1-thio-β-D-glucopranoside

Downstream raw materials:

[(2R,3R,4R,5R,6S)-4,5-Bis-benzyloxy-2-benzyloxymethyl-6-((2R,3R,4S,5R,6S)-4,5-bis-benzyloxy-2-benzyloxymethyl-6-phenylsulfanyl-tetrahydro-pyran-3-yloxy)-tetrahydro-pyran-3-yloxy]-tert-butyl-dimethyl-silane

[(2R,3R,4R,5R,6S)-4,5-Bis-benzyloxy-6-((2R,3S,4R)-4-benzyloxy-2-benzyloxymethyl-3,4-dihydro-2H-pyran-3-yloxy)-2-benzyloxymethyl-tetrahydro-pyran-3-yloxy]-tert-butyl-dimethyl-silane

phenyl(4-O-acetyl-2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-[1-4]-2,3,6-tri-O-benzyl-1-thio-D-glucopyranoside

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 213012-40-9 phenyl 2,3,6-tri-O-benzyl-β-D-glucopyranosyl-[1-4]-2,3,6-tri-O-benzyl-1-thio-β-D-glucopranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send