2-{2-[2-(9H-Fluoren-9-ylmethoxycarbonylamino)-2-methyl-propionylamino]-2-methyl-propionylamino}-2-methyl-propionic acid benzyl ester

Base Information

Chemical Name:2-{2-[2-(9H-Fluoren-9-ylmethoxycarbonylamino)-2-methyl-propionylamino]-2-methyl-propionylamino}-2-methyl-propionic acid benzyl ester
CAS No.:203636-37-7
Molecular Formula:C₃₄H₃₉N₃O₆
Molecular Weight:585.7
Hs Code.:

Synonyms:2-{2-[2-(9H-Fluoren-9-ylmethoxycarbonylamino)-2-methyl-propionylamino]-2-methyl-propionylamino}-2-methyl-propionic acid benzyl ester

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Chemical Property of 2-{2-[2-(9H-Fluoren-9-ylmethoxycarbonylamino)-2-methyl-propionylamino]-2-methyl-propionylamino}-2-methyl-propionic acid benzyl ester

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Technology Process of 2-{2-[2-(9H-Fluoren-9-ylmethoxycarbonylamino)-2-methyl-propionylamino]-2-methyl-propionylamino}-2-methyl-propionic acid benzyl ester

There total 5 articles about 2-{2-[2-(9H-Fluoren-9-ylmethoxycarbonylamino)-2-methyl-propionylamino]-2-methyl-propionylamino}-2-methyl-propionic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94744-50-0
N-[(9H-fluoren-9-ylmethoxy)carbonyl]-α-aminoisobutyric acid

: 203636-37-7
2-{2-[2-(9H-Fluoren-9-ylmethoxycarbonylamino)-2-methyl-propionylamino]-2-methyl-propionylamino}-2-methyl-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / thionyl chloride / CH₂Cl₂ / 24 h

2: 1-hydroxybenzotriazole potassium salt / CH₂Cl₂

With thionyl chloride; 1-Hydroxy-1,2,3-benzotriazole potassium salt; In dichloromethane;
DOI:10.1016/S0040-4039(97)10724-9

Reference yield:

: 55456-40-1
benzyl 2-aminoisobutyrate

: 203636-37-7
2-{2-[2-(9H-Fluoren-9-ylmethoxycarbonylamino)-2-methyl-propionylamino]-2-methyl-propionylamino}-2-methyl-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / diisopropylethyl amine

2: 4-aminomethylpiperidine / 0.5 h

3: 1-hydroxybenzotriazole potassium salt / CH₂Cl₂

With 4-Aminomethylpiperidine; 1-Hydroxy-1,2,3-benzotriazole potassium salt; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4039(97)10724-9

Reference yield:

: 4,4-Dimethyl-2,5-dioxo-oxazolidine-3-carboxylic acid 9H-fluoren-9-ylmethyl ester

: 203636-37-7
2-{2-[2-(9H-Fluoren-9-ylmethoxycarbonylamino)-2-methyl-propionylamino]-2-methyl-propionylamino}-2-methyl-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 35 percent

2: 4-aminomethylpiperidine / 0.5 h

3: 1-hydroxybenzotriazole potassium salt / CH₂Cl₂

With 4-Aminomethylpiperidine; 1-Hydroxy-1,2,3-benzotriazole potassium salt; In dichloromethane;
DOI:10.1016/S0040-4039(97)10724-9