(S)-methyl 3-[(benzo[1,3]dithiole-1,1,3,3-tetraoxide)-2-yl]-3-phenylpropanoate

Base Information

Chemical Name:(S)-methyl 3-[(benzo[1,3]dithiole-1,1,3,3-tetraoxide)-2-yl]-3-phenylpropanoate
CAS No.:1203466-58-3
Molecular Formula:C₁₇H₁₆O₆S₂
Molecular Weight:380.442
Hs Code.:

Synonyms:(S)-methyl 3-[(benzo[1,3]dithiole-1,1,3,3-tetraoxide)-2-yl]-3-phenylpropanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-methyl 3-[(benzo[1,3]dithiole-1,1,3,3-tetraoxide)-2-yl]-3-phenylpropanoate

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Technology Process of (S)-methyl 3-[(benzo[1,3]dithiole-1,1,3,3-tetraoxide)-2-yl]-3-phenylpropanoate

There total 1 articles about (S)-methyl 3-[(benzo[1,3]dithiole-1,1,3,3-tetraoxide)-2-yl]-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1222468-58-7
(S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propionaldehyde

: 18107-18-1
diazomethyl-trimethyl-silane

: 1203466-58-3
(S)-methyl 3-[(benzo[1,3]dithiole-1,1,3,3-tetraoxide)-2-yl]-3-phenylpropanoate

Guidance literature:: (S)-3-phenyl-3-(1,1,3,3-tetraoxo-2,3-dihydro-1H-1λ(6),3λ(6)-benzo[1,3]dithiol-2-yl)-propionaldehyde; With sodium chlorite; potassium dihydrogenphosphate; dihydrogen peroxide; In methanol; water; acetonitrile; at 0 - 20 ℃;

diazomethyl-trimethyl-silane; In methanol; hexane; toluene; optical yield given as %ee;
DOI:10.1002/chem.200902094

Reference yield: 88.0%

: 1203466-58-3
(S)-methyl 3-[(benzo[1,3]dithiole-1,1,3,3-tetraoxide)-2-yl]-3-phenylpropanoate

: 1441-20-9
(R)-(-)-3-phenylbutyric acid methyl ester

Guidance literature:: With chloro-trimethyl-silane; magnesium; ethylene dibromide; In methanol; at 20 ℃; optical yield given as %ee; Inert atmosphere;
DOI:10.1002/chem.200902094