ethyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate

Base Information

• Chemical Name: ethyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate
• CAS No.: 515835-74-2
• Molecular Formula: C₂₅H₂₄O₁₁
• Molecular Weight: 500.459
• Mol file: 515835-74-2.mol

Synonyms:ethyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate

Chemical Property of ethyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate

There total 3 articles about ethyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

3,4,5-triacetoxybenzoyl chloride (70475-59-1) + ethyl ferulate (28028-62-8,74257-26-4,4046-02-0) → ethyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate (515835-74-2)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1016/S0968-0896(01)00361-3

Reference yield:

3,4,5-triacetoxybenzoic acid (6635-24-1) → ethyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate (515835-74-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / SOCl₂ / CHCl₃

2: 87 percent / Et₃N / CH₂Cl₂ / 4 h / 20 °C

With thionyl chloride; triethylamine; In dichloromethane; chloroform;

DOI:10.1016/S0968-0896(01)00361-3

Reference yield:

3,4,5-trihydroxybenzoic acid (149-91-7) → ethyl 3-[4-(3,4,5-triacetyloxybenzoyloxy)-3-methoxyphenyl]-2-propenoate (515835-74-2)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. NaOH

2: 100 percent / SOCl₂ / CHCl₃

3: 87 percent / Et₃N / CH₂Cl₂ / 4 h / 20 °C

With sodium hydroxide; thionyl chloride; triethylamine; In dichloromethane; chloroform;

DOI:10.1016/S0968-0896(01)00361-3

upstream raw materials:

3,4,5-triacetoxybenzoyl chloride

ethyl ferulate

3,4,5-triacetoxybenzoic acid

3,4,5-trihydroxybenzoic acid