4-hydroxy-3-(methoxycarbonyl)benzenediazonium tetrafluoroborate

Base Information

Chemical Name:4-hydroxy-3-(methoxycarbonyl)benzenediazonium tetrafluoroborate
CAS No.:1261270-09-0
Molecular Formula:BF₄*C₈H₇N₂O₃
Molecular Weight:265.96
Hs Code.:

Synonyms:4-hydroxy-3-(methoxycarbonyl)benzenediazonium tetrafluoroborate

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Chemical Property of 4-hydroxy-3-(methoxycarbonyl)benzenediazonium tetrafluoroborate

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Technology Process of 4-hydroxy-3-(methoxycarbonyl)benzenediazonium tetrafluoroborate

There total 2 articles about 4-hydroxy-3-(methoxycarbonyl)benzenediazonium tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 42753-75-3
methyl 5-amino-2-hydroxybenzoate

: 1261270-09-0
4-hydroxy-3-(methoxycarbonyl)benzenediazonium tetrafluoroborate

Guidance literature:: methyl 5-amino-2-hydroxybenzoate; With tetrafluoroboric acid; In water; isopropyl alcohol; at 20 ℃; for 0.5h; Inert atmosphere;

With sodium nitrite; In water; isopropyl alcohol; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/adsc.201000493

Reference yield:

: tetrafluoroboric acid

: 540-80-7
tert.-butylnitrite

: 42753-75-3
methyl 5-amino-2-hydroxybenzoate

: 1261270-09-0
4-hydroxy-3-(methoxycarbonyl)benzenediazonium tetrafluoroborate

Guidance literature:: tetrafluoroboric acid; methyl 5-amino-2-hydroxybenzoate; In tetrahydrofuran; water; at 0 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

tert.-butylnitrite; In tetrahydrofuran; water; at 0 ℃; for 0.5h; Inert atmosphere; Schlenk technique;
DOI:10.1039/d1ob00392e