(+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzoic acid

Base Information

Chemical Name:(+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzoic acid
CAS No.:106485-55-6
Molecular Formula:C₁₆H₁₇NO₆S₂
Molecular Weight:383.446
Hs Code.:

Synonyms:(+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzoic acid

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Chemical Property of (+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzoic acid

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Technology Process of (+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzoic acid

There total 4 articles about (+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 114916-62-0,114916-63-1
2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzoic acid menthyl ester

: 106485-55-6
(+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzoic acid

: 106485-54-5
(-)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzoic acid

Guidance literature:: With sodium hydroxide; In methanol; for 1h; Heating;
DOI:10.1016/S0040-4020(01)86895-2

Reference yield:

: 72856-73-6
2-methoxy-4-(methylsulfanyl)benzoic acid

: 106485-55-6
(+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzoic acid

Guidance literature:: Multi-step reaction with 5 steps

1: thionyl chloride / 2 h / Heating

2: 93 percent / triethylamine / toluene / Heating

3: 89 percent / tetrahydrofuran / 1 h / Heating

4: 23 percent / potassium permanganate / pyridine / 6 h / 50 - 60 °C

5: 50 percent / sodium hydroxide / methanol / 1 h / Heating

With sodium hydroxide; potassium permanganate; thionyl chloride; triethylamine; In tetrahydrofuran; pyridine; methanol; toluene;
DOI:10.1016/S0040-4020(01)86895-2

Reference yield:

: 69883-78-9
2-methoxy-4-(methylthio)benzoyl chloride

: 106485-55-6
(+)-2-methoxy-4-(S-methyl-N-<(4-methylphenyl)-sulfonyl>-sulfonimidoyl)-benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / triethylamine / toluene / Heating

2: 89 percent / tetrahydrofuran / 1 h / Heating

3: 23 percent / potassium permanganate / pyridine / 6 h / 50 - 60 °C

4: 50 percent / sodium hydroxide / methanol / 1 h / Heating

With sodium hydroxide; potassium permanganate; triethylamine; In tetrahydrofuran; pyridine; methanol; toluene;
DOI:10.1016/S0040-4020(01)86895-2