(5-hydroxy-1-ethylpyrazol-4-yl)(3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)phenyl)ketone potassium salt

Base Information

Chemical Name:(5-hydroxy-1-ethylpyrazol-4-yl)(3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)phenyl)ketone potassium salt
CAS No.:1197388-39-8
Molecular Formula:C₁₇H₂₁N₂O₆S*K
Molecular Weight:420.528
Hs Code.:

Synonyms:(5-hydroxy-1-ethylpyrazol-4-yl)(3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)phenyl)ketone potassium salt

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Chemical Property of (5-hydroxy-1-ethylpyrazol-4-yl)(3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)phenyl)ketone potassium salt

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Technology Process of (5-hydroxy-1-ethylpyrazol-4-yl)(3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)phenyl)ketone potassium salt

There total 7 articles about (5-hydroxy-1-ethylpyrazol-4-yl)(3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)phenyl)ketone potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5-hydroxy-1-ethylpyrazol-4-yl 3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)phenyl ketone

: 1197388-39-8
(5-hydroxy-1-ethylpyrazol-4-yl)(3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)phenyl)ketone potassium salt

Guidance literature:: With potassium hydroxide; In methanol; for 1h; Reflux;

Reference yield:

: 1197388-38-7
1-ethyl-1H-pyrazol-5-yl 3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)benzoate

: 1197388-39-8
(5-hydroxy-1-ethylpyrazol-4-yl)(3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)phenyl)ketone potassium salt

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; toluene; for 3h; Reflux; Azeotropic dehydration;

Reference yield:

: 3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)benzoic acid

: 1197388-39-8
(5-hydroxy-1-ethylpyrazol-4-yl)(3-(2-methoxyethoxy)-2-methyl-4-(methylsulfonyl)phenyl)ketone potassium salt

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride / N,N-dimethyl-formamide / chloroform / 3 h / 20 °C

2: triethylamine / toluene / 20 - 80 °C

3: potassium carbonate / N,N-dimethyl-formamide; toluene / 3 h / Reflux; Azeotropic dehydration

With oxalyl dichloride; potassium carbonate; triethylamine; N,N-dimethyl-formamide; In chloroform; N,N-dimethyl-formamide; toluene;