C₂₆H₂₉NO₇S

Base Information

Chemical Name:C₂₆H₂₉NO₇S
CAS No.:1044872-09-4
Molecular Formula:C₂₆H₂₉NO₇S
Molecular Weight:499.585
Hs Code.:

C<sub>26</sub>H<sub>29</sub>NO<sub>7</sub>S

Synonyms:C₂₆H₂₉NO₇S

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Chemical Property of C₂₆H₂₉NO₇S

Chemical Property:

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Technology Process of C₂₆H₂₉NO₇S

There total 6 articles about C₂₆H₂₉NO₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1044872-07-2
C₉H₁₃NO₄S

: 1039885-87-4
C₁₇H₁₈O₄

: 1044872-09-4
C₂₆H₂₉NO₇S

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 24h;

Reference yield:

: 4179-19-5
1,3-dimethoxy-5-methylbenzene

: 1044872-09-4
C₂₆H₂₉NO₇S

Guidance literature:: Multi-step reaction with 4 steps

1: chlorosulfonic acid; carbonic acid dimethyl ester / cyclohexane / 1.25 h / 60 - 72 °C

2: 1,3,5-trichloro-2,4,6-triazine; triethylamine / acetone / 20 h / Heating / reflux

3: ammonia / acetone / 0.5 h / -78 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C

With chlorosulfonic acid; dmap; 1,3,5-trichloro-2,4,6-triazine; ammonia; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; carbonic acid dimethyl ester; In dichloromethane; cyclohexane; acetone;

Reference yield:

: 4919-37-3
3,5-dimethyl-4-hydroxybenzoic acid

: 1044872-09-4
C₂₆H₂₉NO₇S

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 20 °C

1.2: 20 h / 20 °C

2.1: potassium hydroxide; water / tetrahydrofuran; methanol / 24 h / 70 °C

2.2: pH 4 - 5

3.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C

With dmap; potassium hydroxide; water; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;