Technology Process of C19H30N2O3
There total 6 articles about C19H30N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C24H38N2O5;
With
trifluoroacetic acid;
In
dichloromethane;
for 2h;
With
sodium hydroxide;
In
dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: caesium carbonate / dichloromethane / 30 h / 42 °C
2.1: magnesium / iodine / diethyl ether / 2.75 h / Inert atmosphere; Reflux
2.2: 2 h / -78 - 20 °C
2.3: 1 h / 0 - 20 °C
3.1: hydrogenchloride / 1,4-dioxane; methanol / 1.5 h / 20 °C
4.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 16.25 h / 0 - 20 °C
5.1: trifluoroacetic acid / dichloromethane / 2 h
With
hydrogenchloride; benzotriazol-1-ol; caesium carbonate; magnesium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
iodine;
In
1,4-dioxane; methanol; diethyl ether; dichloromethane; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: magnesium / iodine / diethyl ether / 2.75 h / Inert atmosphere; Reflux
1.2: 2 h / -78 - 20 °C
1.3: 1 h / 0 - 20 °C
2.1: hydrogenchloride / 1,4-dioxane; methanol / 1.5 h / 20 °C
3.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 16.25 h / 0 - 20 °C
4.1: trifluoroacetic acid / dichloromethane / 2 h
With
hydrogenchloride; benzotriazol-1-ol; magnesium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
iodine;
In
1,4-dioxane; methanol; diethyl ether; dichloromethane; acetonitrile;