C₅₂H₅₃Cl₂N₅O₁₇

Base Information

• Chemical Name: C₅₂H₅₃Cl₂N₅O₁₇
• CAS No.: 145007-46-1
• Molecular Formula: C₅₂H₅₃Cl₂N₅O₁₇
• Molecular Weight: 1090.92
• Mol file: 145007-46-1.mol

Synonyms:C₅₂H₅₃Cl₂N₅O₁₇

Chemical Property of C₅₂H₅₃Cl₂N₅O₁₇

Chemical Property:

Purity/Quality:

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Technology Process of C₅₂H₅₃Cl₂N₅O₁₇

There total 2 articles about C₅₂H₅₃Cl₂N₅O₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

di-tert-butyl dicarbonate (24424-99-5) + C42H37Cl2N5O13 (145007-45-0) → C52H53Cl2N5O17 (145007-46-1)

Guidance literature:

With sodium hydrogencarbonate; In 1,4-dioxane; water; for 5h; Ambient temperature;

DOI:10.1021/jo9506746

Reference yield:

C58H49Cl2N7O18 → C52H53Cl2N5O17 (145007-46-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) PhNCS, 2.) CF₃CO₂H / 1.) Py, H₂O, room temperature, 7 h, 2.) room temperature, 1.5 h

2: 100 percent / NaHCO₃ / dioxane; H₂O / 5 h / Ambient temperature

With sodium hydrogencarbonate; phenyl isothiocyanate; trifluoroacetic acid; In 1,4-dioxane; water;

DOI:10.1021/jo9506746

Reference yield:

2,2-dimethoxy-propane (77-76-9) + C52H53Cl2N5O17 (145007-46-1) → C55H57Cl2N5O17 (145007-47-2)

Guidance literature:

With toluene-4-sulfonic acid; In acetone; for 1.5h; Ambient temperature;

DOI:10.1021/jo9506746

upstream raw materials:

di-tert-butyl dicarbonate

C₄₂H₃₇Cl₂N₅O₁₃

Downstream raw materials:

C₅₅H₅₇Cl₂N₅O₁₇