dimethyl 3-hydroxy-6-phenylphthalate

Base Information

Chemical Name:dimethyl 3-hydroxy-6-phenylphthalate
CAS No.:194221-01-7
Molecular Formula:C₁₆H₁₄O₅
Molecular Weight:286.284
Hs Code.:

Synonyms:dimethyl 3-hydroxy-6-phenylphthalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethyl 3-hydroxy-6-phenylphthalate

Chemical Property:

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Technology Process of dimethyl 3-hydroxy-6-phenylphthalate

There total 1 articles about dimethyl 3-hydroxy-6-phenylphthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17113-33-6
2-phenylfuran

: 762-42-5
dimethyl acetylenedicarboxylate

: C₁₆H₁₄O₅

: 194221-01-7
dimethyl 3-hydroxy-6-phenylphthalate

Guidance literature:: With iridium(III) chloride trihydrate; In toluene; at 70 ℃; for 48h; Air atmosphere;
DOI:10.1016/j.tetlet.2011.09.068

Reference yield:

: 194221-01-7
dimethyl 3-hydroxy-6-phenylphthalate

: dimethyl 2,2-dimethyl-6-phenyl-2H-chromene-7,8-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 31 percent / K₂CO₃; KI; CuI / dimethylformamide / 2 h / 65 °C

2: 49 percent / dimethylformamide; N,N-dimethyl-aniline / 140 - 150 °C

With copper(l) iodide; potassium carbonate; potassium iodide; In N,N-dimethyl-aniline; N,N-dimethyl-formamide;
DOI:10.1080/10587250008023846