2-Ethyl-2-methyloxane-4-carbothioamide

Base Information

Chemical Name:2-Ethyl-2-methyloxane-4-carbothioamide
CAS No.:84125-27-9
Molecular Formula:C₉H₁₇NOS
Molecular Weight:187.306
Hs Code.:
DSSTox Substance ID:DTXSID701219166
ChEMBL ID:CHEMBL1479190
Mol file:84125-27-9.mol

Synonyms:MLS001047547;SMR000425463;2-Ethyl-2-methyl-tetrahydro-pyran-4-carbothioic acid amide;2-ethyl-2-methyloxane-4-carbothioamide;84125-27-9;CHEMBL1479190;BDBM80255;cid_4366328;DTXSID701219166;HMS2796O15;STK834653;AKOS005623747;2-ethyl-2-methyl-4-oxanecarbothioamide;2-ethyl-2-methyl-oxane-4-carbothioamide;2-ethyl-2-methyl-tetrahydropyran-4-carbothioamide;2-ethyl-2-methyltetrahydro-2H-pyran-4-carbothioamide;2-Ethyltetrahydro-2-methyl-2H-pyran-4-carbothioamide

Suppliers and Price of 2-Ethyl-2-methyloxane-4-carbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Ethyl-2-methyloxane-4-carbothioamide

Chemical Property:

PSA：67.34000
LogP:2.56810
XLogP3:1.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:187.10308534
Heavy Atom Count:12
Complexity:183

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC1(CC(CCO1)C(=S)N)C

Technology Process of 2-Ethyl-2-methyloxane-4-carbothioamide

There total 2 articles about 2-Ethyl-2-methyloxane-4-carbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.9%

: 84125-23-5
2-Ethyl-2-methyl-tetrahydro-pyran-4-carboxylic acid amide

: 84125-27-9
2-Ethyl-2-methyl-tetrahydro-pyran-4-carbothioic acid amide

Guidance literature:: With diphosphorus pentasulfide; In benzene; Heating;
DOI:10.1007/BF00773094

Reference yield:

: 77554-91-7
2-Ethyl-2-methyl-tetrahydro-pyran-4-carbonyl chloride

: 84125-27-9
2-Ethyl-2-methyl-tetrahydro-pyran-4-carbothioic acid amide

Guidance literature:: Multi-step reaction with 2 steps

1: 75.4 percent / NH₃ / diethyl ether / 0.5 h / Ambient temperature

2: 44.9 percent / phosphorus pentasulfide / benzene / Heating

With diphosphorus pentasulfide; ammonia; In diethyl ether; benzene;
DOI:10.1007/BF00773094