N-[2-({[(tert-Butyl)oxy]carbonyl}amino)ethyl]-4,5-dimethyl-2-nitroaniline

Base Information

Chemical Name:N-[2-({[(tert-Butyl)oxy]carbonyl}amino)ethyl]-4,5-dimethyl-2-nitroaniline
CAS No.:261379-89-9
Molecular Formula:C₁₅H₂₃N₃O₄
Molecular Weight:309.365
Hs Code.:

Synonyms:N-[2-({[(tert-Butyl)oxy]carbonyl}amino)ethyl]-4,5-dimethyl-2-nitroaniline

Suppliers and Price of N-[2-({[(tert-Butyl)oxy]carbonyl}amino)ethyl]-4,5-dimethyl-2-nitroaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[2-({[(tert-Butyl)oxy]carbonyl}amino)ethyl]-4,5-dimethyl-2-nitroaniline

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[2-({[(tert-Butyl)oxy]carbonyl}amino)ethyl]-4,5-dimethyl-2-nitroaniline

There total 2 articles about N-[2-({[(tert-Butyl)oxy]carbonyl}amino)ethyl]-4,5-dimethyl-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 610-23-1
4,5-dimethyl-1,2-dinitrobenzene

: 57260-73-8
N-BOC-1,2-diaminoethane

: 261379-89-9
N-[2-({[(tert-Butyl)oxy]carbonyl}amino)ethyl]-4,5-dimethyl-2-nitroaniline

Guidance literature:: In pyridine; at 90 ℃; for 24h;
DOI:10.1002/(SICI)1521-3765(20000103)6:1<62::AID-CHEM62>3.0.CO;2-7

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 261379-89-9
N-[2-({[(tert-Butyl)oxy]carbonyl}amino)ethyl]-4,5-dimethyl-2-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / dioxane / 20 h / 20 °C

2: 67 percent / pyridine / 24 h / 90 °C

In 1,4-dioxane; pyridine; 1: Acylation / 2: ipso-Substitution;
DOI:10.1002/(SICI)1521-3765(20000103)6:1<62::AID-CHEM62>3.0.CO;2-7

Reference yield:

: 261379-89-9
N-[2-({[(tert-Butyl)oxy]carbonyl}amino)ethyl]-4,5-dimethyl-2-nitroaniline

: [2-(2-amino-4,5-dimethyl-phenylamino)-ethyl]-carbamic acid tert-butyl ester

Guidance literature:: With hydrogen; 10percent Pd/C; In methanol; acetic acid; at 20 ℃; for 7h;
DOI:10.1002/(SICI)1521-3765(20000103)6:1<62::AID-CHEM62>3.0.CO;2-7