bis(4-methylbenzenethiolato)[1, 2-bis(diphenylphosphino)ethane]platinum(II)

Base Information

Chemical Name:bis(4-methylbenzenethiolato)[1, 2-bis(diphenylphosphino)ethane]platinum(II)
CAS No.:75365-71-8
Molecular Formula:C₄₀H₃₈P₂PtS₂
Molecular Weight:839.901
Hs Code.:

Synonyms:bis(4-methylbenzenethiolato)[1, 2-bis(diphenylphosphino)ethane]platinum(II)

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Chemical Property of bis(4-methylbenzenethiolato)[1, 2-bis(diphenylphosphino)ethane]platinum(II)

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Technology Process of bis(4-methylbenzenethiolato)[1, 2-bis(diphenylphosphino)ethane]platinum(II)

There total 2 articles about bis(4-methylbenzenethiolato)[1, 2-bis(diphenylphosphino)ethane]platinum(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 83095-83-4,14647-25-7
[platinum(II)dichloride(1,2-bis(diphenylphosphino)ethane)]

: 106-45-6
para-thiocresol

: 75365-71-8
bis(4-methylbenzenethiolato)[1, 2-bis(diphenylphosphino)ethane]platinum(II)

Guidance literature:: With triethylamine; In toluene; (N2); 4-methylbenzenethiol and (C2H5)3N in toluene added dropwise to stirred complex suspn., stirred at room temp. for 19 h; evapd. (vac., room temp.), dissolved in CH2Cl2, washed with H2O, dried (MgSO4), evapd., recrystd. (acetone/hexane); elem. anal.;
DOI:10.1021/ic50216a032

Reference yield: 60.0%

: 83095-83-4,14647-25-7
[platinum(II)dichloride(1,2-bis(diphenylphosphino)ethane)]

: 32812-90-1,68696-14-0
(4-methyl)thiophenolato-lead(II)

: 75365-71-8
bis(4-methylbenzenethiolato)[1, 2-bis(diphenylphosphino)ethane]platinum(II)

Guidance literature:: In acetone; byproducts: PbCl2; N2-atmosphere; recrystn. (Me2CO/hexane); elem. anal.;
DOI:10.1016/S0020-1693(98)00335-1

Reference yield: 81.0%

: Ni(pentafluorophenyl)2(C₆H₅CN)2

: 75365-71-8
bis(4-methylbenzenethiolato)[1, 2-bis(diphenylphosphino)ethane]platinum(II)

: 212518-73-5
Pt(1,2-bis(diphenylphosphanyl)ethane)(SC₆H₄CH₃)2Ni(pentafluorophenyl)2

Guidance literature:: In methanol; addn. of arylthiolate complex to soln. of Ni complex, stirring (room temp., 30 min); concn. (reduced pressure), filtration, washing (hexane), drying (air); elem. anal.;
DOI:10.1002/(SICI)1099-0682(199808)1998:8<1199::AID-EJIC1199>3.0.CO;2-K