(4-methyl)thiophenolato-lead(II)

Base Information

• Chemical Name: (4-methyl)thiophenolato-lead(II)
• CAS No.: 32812-90-1
• Molecular Formula: 2C₇H₇S*Pb
• Molecular Weight: 453.597
• Mol file: 32812-90-1.mol

Synonyms:

Chemical Property of (4-methyl)thiophenolato-lead(II)

Chemical Property:

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (4-methyl)thiophenolato-lead(II)

There total 3 articles about (4-methyl)thiophenolato-lead(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

lead acetate (301-04-2) + para-thiocresol (106-45-6) → (4-methyl)thiophenolato-lead(II) (32812-90-1,68696-14-0)

Guidance literature:

In ethanol; water; dropping of aq. soln. of lead acetate slowly into ethanolic soln. of thio deriv. with stirring under Ar; ppt. stirring at room temp. overnight; filtering, washing with water, ethanol and pentane, drying in vac.;

Reference yield:

lead(II) sulfate + para-thiocresol (106-45-6) → (4-methyl)thiophenolato-lead(II) (32812-90-1,68696-14-0)

Guidance literature:

In water; pptn.;;

Reference yield:

→ (4-methyl)thiophenolato-lead(II) (32812-90-1,68696-14-0)

Guidance literature:

Bleiacetat, p-Tolylthiol;

upstream raw materials:

para-thiocresol

lead acetate

Downstream raw materials:

[Pd2(μ-Stol)2(η(3)-C4H7)2]

[Pd2(μ-Stol)2(η(3)-C3H5)2]

[Pd2Me2(μ-Stol)2(PMe2Ph)2]

bis(4-methylbenzenethiolato)[1, 2-bis(diphenylphosphino)ethane]platinum(II)