6-Acetamido-6-deoxy-ALPHA-D-glucopyranose

Base Information

• Chemical Name: 6-Acetamido-6-deoxy-ALPHA-D-glucopyranose
• CAS No.: 84064-37-9
• Molecular Formula: C₈H₁₅NO₆
• Molecular Weight: 221.21
• Hs Code.: 2932999099
• Mol file: 84064-37-9.mol

Synonyms:6-Acetamido-6-deoxy-α-D-glucopyranose

Chemical Property of 6-Acetamido-6-deoxy-ALPHA-D-glucopyranose

Chemical Property:

• Melting Point: 50 - 52 °C
• PSA: 122.74000
• LogP: -2.23730
• Storage Temp.: ?20°C

Purity/Quality:

97% ^*data from raw suppliers

6-ACETAMIDO-6-DEOXY-ALPHA-D-GLUCOPYRANOSE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-Acetamido-6-deoxy-ALPHA-D-glucopyranose

There total 12 articles about 6-Acetamido-6-deoxy-ALPHA-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

6-acetamide-6-deoxycurdlan → 6-acetamido-6-deoxy-α-D-glucopyranose (84064-37-9)

Guidance literature:

With hydrogenchloride; In water; at 20 ℃; for 48h;

DOI:10.1080/07328303.2014.918624

Reference yield:

D-Glucose (2280-44-6) → 6-acetamido-6-deoxy-α-D-glucopyranose (84064-37-9)

Guidance literature:

Multi-step reaction with 5 steps

1: pyridine / Heating

2: N-bromosuccinimide, triphenylphosphine / dimethylformamide / 3 h / 50 °C

3: sodium azide / dimethylformamide; methanol / 50 °C

4: H₂ / 10percent Pd/C / acetic acid / 6 h / 760 Torr

5: pyridine / 3 h

With N-Bromosuccinimide; sodium azide; hydrogen; triphenylphosphine; palladium on activated charcoal; In pyridine; methanol; acetic acid; N,N-dimethyl-formamide;

DOI:10.1016/0008-6215(85)85063-1

Reference yield:

(2S,3R,4S,5R)-2-Bromomethyl-3,4,5,6-tetrakis-trimethylsilanyloxy-tetrahydro-pyran → 6-acetamido-6-deoxy-α-D-glucopyranose (84064-37-9)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium azide / dimethylformamide; methanol / 50 °C

2: H₂ / 10percent Pd/C / acetic acid / 6 h / 760 Torr

3: pyridine / 3 h

With sodium azide; hydrogen; palladium on activated charcoal; In pyridine; methanol; acetic acid; N,N-dimethyl-formamide;

DOI:10.1016/0008-6215(85)85063-1

upstream raw materials:

methyl-(6-acetylamino-6-deoxy-α-D-glucopyranoside)

acetic anhydride

Methyl-2,3,5-triacetyl-β-D-glucofuranuronsaeurenitril

Benzyl-2,3,5-triacetyl-β-D-glucofuranuronsaeurenitril