2,5-di(anthracen-2-yl)-1-methyl-1,3,4-triphenylsilole

Base Information

Chemical Name:2,5-di(anthracen-2-yl)-1-methyl-1,3,4-triphenylsilole
CAS No.:1593560-78-1
Molecular Formula:C₅₁H₃₆Si
Molecular Weight:676.932
Hs Code.:

Synonyms:2,5-di(anthracen-2-yl)-1-methyl-1,3,4-triphenylsilole

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Chemical Property of 2,5-di(anthracen-2-yl)-1-methyl-1,3,4-triphenylsilole

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Technology Process of 2,5-di(anthracen-2-yl)-1-methyl-1,3,4-triphenylsilole

There total 2 articles about 2,5-di(anthracen-2-yl)-1-methyl-1,3,4-triphenylsilole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 7321-27-9
2-bromoanthracene

: 23024-19-3
bis(phenylethynylene)methylphenylsilane

: 1593560-78-1
2,5-di(anthracen-2-yl)-1-methyl-1,3,4-triphenylsilole

Guidance literature:: bis(phenylethynylene)methylphenylsilane; With naphthalene; lithium; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

With zinc dichloro(N,N,N′,N′-tetramethylethylenediamine); In tetrahydrofuran; at -10 - 20 ℃; for 1h; Inert atmosphere;

2-bromoanthracene; With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; for 12h; Reflux; Inert atmosphere;
DOI:10.1039/c4cc00653d

Reference yield:

: 536-74-3
phenylacetylene

: 1593560-78-1
2,5-di(anthracen-2-yl)-1-methyl-1,3,4-triphenylsilole

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium

2.1: naphthalene; lithium / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2.2: 1 h / -10 - 20 °C / Inert atmosphere

2.3: 12 h / Reflux; Inert atmosphere

With n-butyllithium; naphthalene; lithium; In tetrahydrofuran;
DOI:10.1039/c4cc00653d