1,4-bis(2-pyridylmethyl)-7-((4-(1,3-benzothiazol-2-yl)phenylamino)-2-oxoethyl)-1,4,7-triazacyclononane

Base Information

Chemical Name:1,4-bis(2-pyridylmethyl)-7-((4-(1,3-benzothiazol-2-yl)phenylamino)-2-oxoethyl)-1,4,7-triazacyclononane
CAS No.:1430238-23-5
Molecular Formula:C₃₃H₃₅N₇OS
Molecular Weight:577.753
Hs Code.:

Synonyms:1,4-bis(2-pyridylmethyl)-7-((4-(1,3-benzothiazol-2-yl)phenylamino)-2-oxoethyl)-1,4,7-triazacyclononane

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Chemical Property of 1,4-bis(2-pyridylmethyl)-7-((4-(1,3-benzothiazol-2-yl)phenylamino)-2-oxoethyl)-1,4,7-triazacyclononane

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Technology Process of 1,4-bis(2-pyridylmethyl)-7-((4-(1,3-benzothiazol-2-yl)phenylamino)-2-oxoethyl)-1,4,7-triazacyclononane

There total 8 articles about 1,4-bis(2-pyridylmethyl)-7-((4-(1,3-benzothiazol-2-yl)phenylamino)-2-oxoethyl)-1,4,7-triazacyclononane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 159221-73-5
1,4-bis(pyridin-2-ylmethyl)-1,4,7-triazacyclononane

: 182274-80-2
N-(4-(1,3-benzothiazol-2-yl)phenyl)-2-chloroacetamide

: 1430238-23-5
1,4-bis(2-pyridylmethyl)-7-((4-(1,3-benzothiazol-2-yl)phenylamino)-2-oxoethyl)-1,4,7-triazacyclononane

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile; for 72h; Inert atmosphere; Reflux;
DOI:10.1016/j.poly.2012.10.029

Reference yield:

: 4377-33-7
2-chloromethylpyridine

: 1430238-23-5
1,4-bis(2-pyridylmethyl)-7-((4-(1,3-benzothiazol-2-yl)phenylamino)-2-oxoethyl)-1,4,7-triazacyclononane

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

2: water / Heating

3: potassium carbonate; potassium iodide / acetonitrile / 120 h / Inert atmosphere; Heating

4: hydrogenchloride / 24 h / 20 °C

5: potassium carbonate; potassium iodide / acetonitrile / 72 h / Inert atmosphere; Reflux

With hydrogenchloride; water; potassium carbonate; potassium iodide; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.poly.2012.10.029

Reference yield:

: 1011533-84-8
1-(2-pyridylmethyl)-4-formyl-1,4,7-triazacyclononane

: 1430238-23-5
1,4-bis(2-pyridylmethyl)-7-((4-(1,3-benzothiazol-2-yl)phenylamino)-2-oxoethyl)-1,4,7-triazacyclononane

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; potassium iodide / acetonitrile / 120 h / Inert atmosphere; Heating

2: hydrogenchloride / 24 h / 20 °C

3: potassium carbonate; potassium iodide / acetonitrile / 72 h / Inert atmosphere; Reflux

With hydrogenchloride; potassium carbonate; potassium iodide; In acetonitrile;
DOI:10.1016/j.poly.2012.10.029