(3S)-1-benzyloxycarbonyl-3-(tert-butoxycarbonyl)amino-4-(1-hydroxy-1-methyl)ethylpyrrolidine

Base Information

Chemical Name:(3S)-1-benzyloxycarbonyl-3-(tert-butoxycarbonyl)amino-4-(1-hydroxy-1-methyl)ethylpyrrolidine
CAS No.:869956-14-9
Molecular Formula:C₂₀H₃₀N₂O₅
Molecular Weight:378.469
Hs Code.:

Synonyms:(3S)-1-benzyloxycarbonyl-3-(tert-butoxycarbonyl)amino-4-(1-hydroxy-1-methyl)ethylpyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S)-1-benzyloxycarbonyl-3-(tert-butoxycarbonyl)amino-4-(1-hydroxy-1-methyl)ethylpyrrolidine

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Technology Process of (3S)-1-benzyloxycarbonyl-3-(tert-butoxycarbonyl)amino-4-(1-hydroxy-1-methyl)ethylpyrrolidine

There total 1 articles about (3S)-1-benzyloxycarbonyl-3-(tert-butoxycarbonyl)amino-4-(1-hydroxy-1-methyl)ethylpyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 869956-13-8
(3S,4S)-1-Benzyloxycarbonyl-3-(tert-butoxycarbonyl)amino-4-methoxycarbonylpyrrolidine

: 75-16-1
methylmagnesium bromide

: 869956-14-9
(3S)-1-benzyloxycarbonyl-3-(tert-butoxycarbonyl)amino-4-(1-hydroxy-1-methyl)ethylpyrrolidine

Guidance literature:: (3S,4S)-1-Benzyloxycarbonyl-3-(tert-butoxycarbonyl)amino-4-methoxycarbonylpyrrolidine; methylmagnesium bromide; In tetrahydrofuran; at -10 ℃; for 0.333333h;

With water; ammonium chloride; In tetrahydrofuran; for 0.5h;

Reference yield: 47.0%

: 869956-14-9
(3S)-1-benzyloxycarbonyl-3-(tert-butoxycarbonyl)amino-4-(1-hydroxy-1-methyl)ethylpyrrolidine

: 869956-15-0
(3S)-1-(Benzyloxycarbonyl)-3-(tert-butoxycarbonyl)amino-4-isopropenylpyrrolidine

Guidance literature:: (3S)-1-benzyloxycarbonyl-3-(tert-butoxycarbonyl)amino-4-(1-hydroxy-1-methyl)ethylpyrrolidine; With dmap; methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 12h;

With water; ammonium chloride; In dichloromethane; at 0 ℃;