(2S,3S)-ethyl 3-((S)-2-(N-allylbenzamido)propanamido)-6-((2-methoxyethoxy)methoxy)-2,3-dihydrobenzo furan-2-carboxylate

Base Information

Chemical Name:(2S,3S)-ethyl 3-((S)-2-(N-allylbenzamido)propanamido)-6-((2-methoxyethoxy)methoxy)-2,3-dihydrobenzo furan-2-carboxylate
CAS No.:1592907-44-2
Molecular Formula:C₂₈H₃₄N₂O₈
Molecular Weight:526.587
Hs Code.:

Synonyms:(2S,3S)-ethyl 3-((S)-2-(N-allylbenzamido)propanamido)-6-((2-methoxyethoxy)methoxy)-2,3-dihydrobenzo furan-2-carboxylate

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Chemical Property of (2S,3S)-ethyl 3-((S)-2-(N-allylbenzamido)propanamido)-6-((2-methoxyethoxy)methoxy)-2,3-dihydrobenzo furan-2-carboxylate

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Technology Process of (2S,3S)-ethyl 3-((S)-2-(N-allylbenzamido)propanamido)-6-((2-methoxyethoxy)methoxy)-2,3-dihydrobenzo furan-2-carboxylate

There total 1 articles about (2S,3S)-ethyl 3-((S)-2-(N-allylbenzamido)propanamido)-6-((2-methoxyethoxy)methoxy)-2,3-dihydrobenzo furan-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 958138-35-7
C₁₅H₂₁NO₆

: 1592907-28-2
C₁₃H₁₅NO₃

: 1592907-44-2
(2S,3S)-ethyl 3-((S)-2-(N-allylbenzamido)propanamido)-6-((2-methoxyethoxy)methoxy)-2,3-dihydrobenzo furan-2-carboxylate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.201301769 DOI:10.1002/ejoc.201301769

Reference yield:

: 1592907-44-2
(2S,3S)-ethyl 3-((S)-2-(N-allylbenzamido)propanamido)-6-((2-methoxyethoxy)methoxy)-2,3-dihydrobenzo furan-2-carboxylate

: 1592907-74-8
N-allyl-N-((S)-1-((2S,3S)-2-(allyloxymethyl)-6-((2-methoxyethoxy)methoxy)-2,3-dihydrobenzofuran-3-ylamino)-1-oxopropan-2-yl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium borohydride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

2.2: 6 h / 0 °C / Inert atmosphere

With lithium borohydride; sodium hydride; In tetrahydrofuran;
DOI:10.1002/ejoc.201301769

Reference yield:

: 1592907-44-2
(2S,3S)-ethyl 3-((S)-2-(N-allylbenzamido)propanamido)-6-((2-methoxyethoxy)methoxy)-2,3-dihydrobenzo furan-2-carboxylate

: 1592907-89-5
(3S,10aS,15bS,E)-4-benzoyl-13-((2-methoxyethoxy)methoxy)-3-methyl-4,5,8,10,10a,15b-hexahydro-1H-benzofuro[2,3-c][1,5,8]oxadiazacyclododecin-2(3H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium borohydride / tetrahydrofuran / 3 h / 0 - 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 0.08 h / 0 °C / Inert atmosphere

2.2: 6 h / 0 °C / Inert atmosphere

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 20 °C / Inert atmosphere; Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; lithium borohydride; sodium hydride; In tetrahydrofuran; dichloromethane;
DOI:10.1002/ejoc.201301769