(3R,4S) 3-(benzyloxycarbonylamino)-4-(tertbutoxycarbonylamino)-5-methylhexanoic acid

Base Information

Chemical Name:(3R,4S) 3-(benzyloxycarbonylamino)-4-(tertbutoxycarbonylamino)-5-methylhexanoic acid
CAS No.:1263315-51-0
Molecular Formula:C₂₀H₃₀N₂O₆
Molecular Weight:394.468
Hs Code.:

Synonyms:(3R,4S) 3-(benzyloxycarbonylamino)-4-(tertbutoxycarbonylamino)-5-methylhexanoic acid

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Chemical Property of (3R,4S) 3-(benzyloxycarbonylamino)-4-(tertbutoxycarbonylamino)-5-methylhexanoic acid

Chemical Property:

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Technology Process of (3R,4S) 3-(benzyloxycarbonylamino)-4-(tertbutoxycarbonylamino)-5-methylhexanoic acid

There total 12 articles about (3R,4S) 3-(benzyloxycarbonylamino)-4-(tertbutoxycarbonylamino)-5-methylhexanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1263315-49-6
(2S,3R)-tert-butyl 3-(benzyloxycarbonylamino)-2-isopropyl-5-oxopyrrolidine-1-carboxylate

: 1263315-51-0
(3R,4S) 3-(benzyloxycarbonylamino)-4-(tertbutoxycarbonylamino)-5-methylhexanoic acid

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; Inert atmosphere;
DOI:10.1039/c2ob26828k

Reference yield:

: 1263485-59-1
C₇H₁₄N₂O*ClH

: 1263315-51-0
(3R,4S) 3-(benzyloxycarbonylamino)-4-(tertbutoxycarbonylamino)-5-methylhexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / water; methanol / Inert atmosphere

2: triethylamine; dmap / dichloromethane / Inert atmosphere

3: lithium hydroxide; water / tetrahydrofuran / Inert atmosphere

With dmap; water; sodium hydrogencarbonate; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c2ob26828k

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1263315-51-0
(3R,4S) 3-(benzyloxycarbonylamino)-4-(tertbutoxycarbonylamino)-5-methylhexanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / water; methanol / Inert atmosphere

2: triethylamine; dmap / dichloromethane / Inert atmosphere

3: lithium hydroxide; water / tetrahydrofuran / Inert atmosphere

With dmap; water; sodium hydrogencarbonate; triethylamine; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1039/c2ob26828k