4-t-butylcyclohexanone di-t-butylacetal

Base Information

• Chemical Name: 4-t-butylcyclohexanone di-t-butylacetal
• CAS No.: 122851-16-5
• Molecular Formula: C₁₈H₃₆O₂
• Molecular Weight: 284.483
• Mol file: 122851-16-5.mol

Synonyms:4-t-butylcyclohexanone di-t-butylacetal

Chemical Property of 4-t-butylcyclohexanone di-t-butylacetal

Chemical Property:

Purity/Quality:

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Technology Process of 4-t-butylcyclohexanone di-t-butylacetal

There total 2 articles about 4-t-butylcyclohexanone di-t-butylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

4-(1,1-dimethylethyl)-cyclohexanol (98-52-2) → 4-t-butylcyclohexanone di-t-butylacetal (122851-16-5) + 4-tercbutyl-cyclohexanone (98-53-3)

Guidance literature:

With sodium bromate; cerium; In benzene; at 80 ℃; for 1.5h;

DOI:10.1246/bcsj.62.519

Reference yield: 30.0%

tert.-butylhydroperoxide (75-91-2) + 4-(1,1-dimethylethyl)-cyclohexanol (98-52-2) → 4-t-butylcyclohexanone di-t-butylacetal (122851-16-5) + 4-tercbutyl-cyclohexanone (98-53-3)

Guidance literature:

Ce(IV) impregnated Nafion^R 511; hydrogen cation; in presence of NaHCO₃;

DOI:10.1016/S0040-4039(01)81373-3

upstream raw materials:

tert.-butylhydroperoxide

4-(1,1-dimethylethyl)-cyclohexanol