(2R,4S,5S,6S)-7-benzyloxy-5-hydroxy-2,4,6-trimethylheptanoic acid δ-lactone

Base Information

Chemical Name:(2R,4S,5S,6S)-7-benzyloxy-5-hydroxy-2,4,6-trimethylheptanoic acid δ-lactone
CAS No.:144606-47-3
Molecular Formula:C₁₇H₂₄O₃
Molecular Weight:276.376
Hs Code.:

Synonyms:(2R,4S,5S,6S)-7-benzyloxy-5-hydroxy-2,4,6-trimethylheptanoic acid δ-lactone

Suppliers and Price of (2R,4S,5S,6S)-7-benzyloxy-5-hydroxy-2,4,6-trimethylheptanoic acid δ-lactone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (2R,4S,5S,6S)-7-benzyloxy-5-hydroxy-2,4,6-trimethylheptanoic acid δ-lactone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2R,4S,5S,6S)-7-benzyloxy-5-hydroxy-2,4,6-trimethylheptanoic acid δ-lactone

There total 12 articles about (2R,4S,5S,6S)-7-benzyloxy-5-hydroxy-2,4,6-trimethylheptanoic acid δ-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: (3R,5S,6S)-6-((S)-2-Benzyloxy-1-methyl-ethyl)-3,5-dimethyl-tetrahydro-pyran-2-ol

: 144606-47-3
(2R,4S,5S,6S)-7-benzyloxy-5-hydroxy-2,4,6-trimethylheptanoic acid δ-lactone

Guidance literature:: With 3 A molecular sieve; pyridinium chlorochromate; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/0040-4020(95)00905-1

Reference yield:

: 94743-00-7,94743-01-8,135030-18-1,135030-19-2,144665-39-4
(5S,6S)-6-((S)-2-Benzyloxy-1-methyl-ethyl)-5-methyl-tetrahydro-pyran-2-one

: 74-88-4
methyl iodide

: 94743-02-9,94743-03-0,144606-47-3
(3S,5S,6S)-6-((S)-2-Benzyloxy-1-methyl-ethyl)-3,5-dimethyl-tetrahydro-pyran-2-one

: 94743-02-9,94743-03-0,144606-47-3
(3R,5S,6S)-6-((S)-2-Benzyloxy-1-methyl-ethyl)-3,5-dimethyl-tetrahydro-pyran-2-one

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(01)90179-0

Reference yield:

: 94743-00-7,94743-01-8,135030-18-1,135030-19-2,144665-39-4
(5S,6S)-6-((S)-2-Benzyloxy-1-methyl-ethyl)-5-methyl-tetrahydro-pyran-2-one

: 74-88-4
methyl iodide

: 94743-02-9,94743-03-0,144606-47-3
(3S,5S,6S)-6-((S)-2-Benzyloxy-1-methyl-ethyl)-3,5-dimethyl-tetrahydro-pyran-2-one

: 94743-02-9,94743-03-0,144606-47-3
(3R,5S,6S)-6-((S)-2-Benzyloxy-1-methyl-ethyl)-3,5-dimethyl-tetrahydro-pyran-2-one

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; Yield given. Yields of byproduct given;
DOI:10.1016/S0040-4039(01)90179-0