Technology Process of C15H21N5O4
There total 5 articles about C15H21N5O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine;
In
di-isopropyl ether;
at 45 ℃;
for 2h;
Solvent;
DOI:10.1016/j.tetlet.2014.06.027
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trifluoroacetic acid / dichloromethane / 20 °C
2: Candida antarctica lipase B / tert-butyl methyl ether / 72 h / 40 °C / Enzymatic reaction
With
Candida antarctica lipase B; trifluoroacetic acid;
In
dichloromethane; tert-butyl methyl ether;
DOI:10.1016/j.tetlet.2014.06.027
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: triethylamine / tetrahydrofuran
2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran
3.1: diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 20 °C
3.2: 80 °C
4.1: trifluoroacetic acid / dichloromethane / 20 °C
5.1: Candida antarctica lipase B / tert-butyl methyl ether / 72 h / 40 °C / Enzymatic reaction
With
Candida antarctica lipase B; diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 9-bora-bicyclo[3.3.1]nonane; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; tert-butyl methyl ether; toluene;
DOI:10.1016/j.tetlet.2014.06.027