diethyl {4-[N-(phenyl)amino-(diethoxyphosphoryl)methyl]phenyl}-N-(phenyl)aminomethylphosphonate

Base Information

Chemical Name:diethyl {4-[N-(phenyl)amino-(diethoxyphosphoryl)methyl]phenyl}-N-(phenyl)aminomethylphosphonate
CAS No.:13336-77-1
Molecular Formula:C₂₈H₃₈N₂O₆P₂
Molecular Weight:560.567
Hs Code.:

Synonyms:diethyl {4-[N-(phenyl)amino-(diethoxyphosphoryl)methyl]phenyl}-N-(phenyl)aminomethylphosphonate

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Chemical Property of diethyl {4-[N-(phenyl)amino-(diethoxyphosphoryl)methyl]phenyl}-N-(phenyl)aminomethylphosphonate

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Technology Process of diethyl {4-[N-(phenyl)amino-(diethoxyphosphoryl)methyl]phenyl}-N-(phenyl)aminomethylphosphonate

There total 8 articles about diethyl {4-[N-(phenyl)amino-(diethoxyphosphoryl)methyl]phenyl}-N-(phenyl)aminomethylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 623-27-8
terephthalaldehyde,

: 62-53-3
aniline

: 762-04-9
phosphonic acid diethyl ester

: 13336-77-1
diethyl {4-[N-(phenyl)amino-(diethoxyphosphoryl)methyl]phenyl}-N-(phenyl)aminomethylphosphonate

Guidance literature:: With sodium dodecyl-sulfate; In water; at 50 ℃; for 0.25h; Micellar solution;
DOI:10.1055/s-0029-1216789

Reference yield: 93.0%

: 100-52-7
benzaldehyde

: 762-04-9
phosphonic acid diethyl ester

: 106-50-3
1,4-phenylenediamine

: 13336-77-1
diethyl {4-[N-(phenyl)amino-(diethoxyphosphoryl)methyl]phenyl}-N-(phenyl)aminomethylphosphonate

Guidance literature:: With xanthan sulfuric acid; at 60 ℃; for 1h; Neat (no solvent);
DOI:10.1002/jccs.201000194

Reference yield: 92.0%

: 623-27-8
terephthalaldehyde,

: 62-53-3
aniline

: 122-52-1
triethyl phosphite

: 13336-77-1
diethyl {4-[N-(phenyl)amino-(diethoxyphosphoryl)methyl]phenyl}-N-(phenyl)aminomethylphosphonate

Guidance literature:: With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; In dichloromethane; ethyl acetate; at 26 ℃; for 2h; Optical yield = 10 %de;
DOI:10.1002/hc.21170