C₂₃H₃₃NO₇

Base Information

• Chemical Name: C₂₃H₃₃NO₇
• CAS No.: 1155868-23-7
• Molecular Formula: C₂₃H₃₃NO₇
• Molecular Weight: 435.518
• Mol file: 1155868-23-7.mol

Synonyms:C₂₃H₃₃NO₇

Chemical Property of C₂₃H₃₃NO₇

Chemical Property:

Purity/Quality:

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Technology Process of C₂₃H₃₃NO₇

There total 2 articles about C₂₃H₃₃NO₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

(S)-benzyl 5-(dihydroxymethyl)-2,2-dimethyloxazolidine-3-carboxylate (1155868-20-4) + 2-tert-butyl-2-methyl-1,3-dioxan-5-one (170876-75-2) → C23H33NO7 (1155868-23-7)

Guidance literature:

With L-proline; lithium chloride; In dimethyl sulfoxide; at 5 - 20 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;

DOI:10.1021/jo900263s

Reference yield:

(S)-benzyl 5-(dihydroxymethyl)-2,2-dimethyloxazolidine-3-carboxylate (1155868-20-4) + 2-tert-butyl-2-methyl-1,3-dioxan-5-one (170876-75-2) → C23H33NO7 (1155868-23-7) + C23H33NO7 (1155868-37-3)

Guidance literature:

With D-Prolin; lithium bromide; In dimethyl sulfoxide; at 4 ℃; for 96h; Overall yield = 58 %;

DOI:10.1016/j.tetasy.2012.07.012

upstream raw materials:

(S)-benzyl 5-(dihydroxymethyl)-2,2-dimethyloxazolidine-3-carboxylate

2-tert-butyl-2-methyl-1,3-dioxan-5-one