α-tert-butyl N--n-butylamine

Base Information

Chemical Name:α-tert-butyl N--n-butylamine
CAS No.:95063-74-4
Molecular Formula:C₂₁H₃₂N₂O₅
Molecular Weight:392.495
Hs Code.:

α-tert-butyl N-<N-(benzyloxycarbonyl)-L-γ-glutamyl>-n-butylamine

Synonyms:α-tert-butyl N--n-butylamine

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Chemical Property of α-tert-butyl N--n-butylamine

Chemical Property:

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Technology Process of α-tert-butyl N--n-butylamine

There total 2 articles about α-tert-butyl N--n-butylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5891-45-2
(S)-2-(benzyloxycarbonylamino)pentanedioic acid tert-butyl ester

: 109-73-9,85404-21-3
N-butylamine

: 95063-74-4
α-tert-butyl N--n-butylamine

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; Yield given. Multistep reaction; 1.) THF, -20 deg C, 10 min, 2.) THF, a) -20 deg C, 10 min, b) from -20 deg to RT;
DOI:10.1021/jm00046a014

Reference yield:

: 540-88-5
acetic acid tert-butyl ester

: 1155-62-0
N-benzyloxycarbonyl-L-glutamic acid

: 109-73-9,85404-21-3
N-butylamine

: 95063-73-3
(S)-4-Benzyloxycarbonylamino-4-butylcarbamoyl-butyric acid tert-butyl ester

: 95063-74-4
α-tert-butyl N--n-butylamine

Guidance literature:: Yield given. Multistep reaction;

Reference yield:

: 95063-74-4
α-tert-butyl N--n-butylamine

: 161879-08-9
tert-butyl N--N-prop-2-ynylamino>benzoyl>-L-γ-glutamyl>-n-butylamide

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / tetrahydrofuran / 4 h / 760 Torr

2: 80 percent / diethyl cyanophosphoridate, Et₃N / dimethylformamide / 2 h / Ambient temperature

With diethyl cyanophosphoridate; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm00046a014