(E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)propanoic acid

Base Information

Chemical Name:(E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)propanoic acid
CAS No.:1092557-65-7
Molecular Formula:C₁₄H₁₂O₆
Molecular Weight:276.246
Hs Code.:

Synonyms:(E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)propanoic acid

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Chemical Property of (E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)propanoic acid

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Technology Process of (E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)propanoic acid

There total 3 articles about (E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1092557-64-6
methyl (E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)propanoate

: 1092557-65-7
(E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)propanoic acid

Guidance literature:: methyl (E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)propanoate; With sodium hydroxide; In water; for 0.5h; Reflux;

With hydrogenchloride; In water; pH=1;
DOI:10.1021/jo801817s

Reference yield: 83.0%

: 1092557-61-3
3-(4-methoxyphenyl)-6-methylfuro[3,2-b]furan-2,5-dione

: 67-63-0,8013-70-5
isopropyl alcohol

: 1092557-65-7
(E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)propanoic acid

: 1092557-68-0
isopropyl (E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)propanoate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -78 ℃; for 0.25h; regioselective reaction;
DOI:10.1021/jo801817s

Reference yield: 78.0%

: 1146510-10-2
Methyl 2-(3-methoxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-propanoate

: 1092557-65-7
(E)-2-(3-hydroxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)propanoic acid

Guidance literature:: Methyl 2-(3-methoxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-propanoate; With magnesium bromide; In N,N-dimethyl-formamide; at 120 ℃; for 5h;

With water; optical yield given as %de;
DOI:10.1002/cmdc.201000391