Methyl 2-(3-methoxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-propanoate

Base Information

Chemical Name:Methyl 2-(3-methoxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-propanoate
CAS No.:1146510-10-2
Molecular Formula:C₁₆H₁₆O₆
Molecular Weight:304.299
Hs Code.:

Synonyms:Methyl 2-(3-methoxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-propanoate

Suppliers and Price of Methyl 2-(3-methoxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 2-(3-methoxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-propanoate

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Technology Process of Methyl 2-(3-methoxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-propanoate

There total 3 articles about Methyl 2-(3-methoxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 58368-11-9
4-Methoxy-3-(4-methoxyphenyl)-furan-2(5H)-one

: 600-22-6
pyruvic acid methyl ester

: 1146510-10-2
Methyl 2-(3-methoxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-propanoate

Guidance literature:: With dmap; n-butyllithium; ammonium chloride; triethylamine; diisopropylamine; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.ica.2012.08.009

Reference yield:

: 1092557-62-4
C₁₆H₁₈O₇

: 1146510-10-2
Methyl 2-(3-methoxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-propanoate

Guidance literature:: With dmap; triethylamine; trifluoroacetic anhydride; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jo801817s

Reference yield:

: 23786-14-3
4-methoxy-phenyl acetic acid methyl ester

: 1146510-10-2
Methyl 2-(3-methoxy-4-(4-methoxyphenyl)-5-oxofuran-2(5H)-ylidene)-propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride; potassium tert-butylate

2: potassium carbonate / acetone / 4 h / Reflux

3: diisopropylamine; n-butyllithium; ammonium chloride; triethylamine; dmap; trifluoroacetic anhydride / tetrahydrofuran; dichloromethane

With hydrogenchloride; dmap; n-butyllithium; ammonium chloride; potassium tert-butylate; potassium carbonate; triethylamine; diisopropylamine; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.ica.2012.08.009